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0 0 6.3192 142.14 692.4 Tm (\(a\))Tj /TT0 1 Tf 0 Tc 10.2735 4.3676 Td ( )Tj -0.00079 Tc -0.00169 Tw 0 6.3192 -6.3192 0 108 625.8 Tm [(Cu)-4.8 (r)-9.6 (r)-0.1 (e)-4.8 (n)-14.3 (t / )-9.5 (mA)]TJ 0.0049 Tc -0.0074 Tw 6.3192 0 0 6.3192 157.74 565.8 Tm [(Pot)7.4 (ent)7.4 (ial /)7.4 ( V)7.3 ( )]TJ /TT2 1 Tf -0.0063 Tc 0 Tw 5.6969 0 Td [(ve)-19.8 (r)-5.6 (s)-9.5 (u)-10.3 (s)]TJ /TT0 1 Tf -0.0024 Tc -0.00011 Tw 2.9624 0 Td [( Ag)-6.4 (/A)-9.5 (g)-6.4 (C)-1.8 (l)-8.1 (/)0.1 (KC)-11.3 (l)]TJ 0.00011 Tc 0 Tw 3.7781 0 0 3.7781 249.42 563.34 Tm [(\(s)-8.1 (at)8 (.)-7.9 (\))]TJ ET 1 0 0 1 226.44 639.42 cm 0 0 m 14.52 0 l S 1 0 0 1 -226.44 -639.42 cm BT /TT0 1 Tf -0.005 Tc 5.7173 0 0 5.7173 240.96 637.5 Tm [( f)-10.5 (i)-3.2 (r)-7.8 (s)-8.7 (t )-10.5 (s)-8.7 (c)-8.7 (a)-5 (n)]TJ ET 1 0 0 1 226.44 632.4 cm 0 0 m 0.78 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.8 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.48 0 l S 1 0 0 1 -240.42 -632.4 cm BT /TT0 1 Tf 0.0049 Tc -0.0099 Tw 5.7173 0 0 5.7173 240.96 630.48 Tm [( fi)6.7 (fth)15.3 ( )-10.5 (sca)4.9 (n)]TJ ET 1 0 0 1 226.44 625.44 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 -240.48 -625.44 cm BT /TT0 1 Tf -0.00031 Tc -0.0047 Tw 5.7173 0 0 5.7173 240.96 623.52 Tm [( t)-5.8 (enth )-10.5 (scan)]TJ ET 1 0 0 1 226.44 618.48 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.18 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.96 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.18 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.96 0 l S 1 0 0 1 -239.88 -618.48 cm BT /TT0 1 Tf 0.005 Tc -0.00999 Tw 5.7173 0 0 5.7173 240.96 616.5 Tm [( fi)6.8 (fte)15.4 (e)4.9 (n)5 (th)5 ( sca)5 (n)]TJ ET 1 0 0 1 226.44 611.46 cm 0 0 m 0.72 0 l S 1 0 0 1 1.2 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.72 0 l S 1 0 0 1 1.2 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.18 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.72 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.18 0 l S 1 0 0 1 0.66 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.72 0 l S 1 0 0 1 1.2 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.72 0 l S 1 0 0 1 -239.88 -611.46 cm BT /TT0 1 Tf 0.0047 Tc -0.0097 Tw 5.7173 0 0 5.7173 240.96 609.54 Tm [( tw)13.2 (e)4.7 (n)15.1 (ty)11.5 (-fi)6.5 (f)-0.8 (t)9.7 (h)4.6 ( )-10.5 (sca)4.7 (n)]TJ ET 1 0 0 1 226.44 604.5 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.42 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.42 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.84 0 cm 0 0 m 0.36 0 l S 1 0 0 1 0.78 0 cm 0 0 m 0.36 0 l S 1 0 0 1 -240.36 -604.5 cm BT /TT0 1 Tf 0.00481 Tc 5.7173 0 0 5.7173 240.96 602.52 Tm [( th)4.8 (i)6.6 (r)2 (t)9.8 (y)1.1 (-)12.5 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1 0 0 1 -0.72 -0.06 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.78 0 l S 1 0 0 1 -1.26 0 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.18 0 l -0.18 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.78 0 l S 1 0 0 1 -1.26 -0.06 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.66 0 cm 0 0 m -0.18 0 l -0.24 0 l S 1 0 0 1 -0.78 -0.06 cm 0 0 m -0.72 -0.06 l S 1 0 0 1 -1.26 -0.06 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.66 -0.06 cm 0 0 m -0.12 0 l -0.24 0 l S 1 0 0 1 -0.78 0 cm 0 0 m -0.72 -0.12 l S 1 0 0 1 -1.2 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.06 0 l -0.24 0 l S 1 0 0 1 -0.78 -0.06 cm 0 0 m -0.72 -0.06 l S 1 0 0 1 -1.2 -0.12 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m 0 0 l -0.24 0 l S 1 0 0 1 -0.78 -0.06 cm 0 0 m -0.72 -0.12 l S 1 0 0 1 -1.2 -0.18 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.78 -0.12 cm 0 0 m -0.72 -0.06 l S 1 0 0 1 -1.2 -0.18 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.78 -0.12 cm 0 0 m -0.72 -0.12 l S 1 0 0 1 -1.2 -0.18 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.78 -0.06 cm 0 0 m -0.72 -0.12 l S 1 0 0 1 -1.2 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.78 -0.12 l S 1 0 0 1 -1.26 -0.18 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.78 -0.12 l S 1 0 0 1 -1.26 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.18 cm 0 0 m -0.78 -0.06 l S 1 0 0 1 -1.26 -0.18 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.18 cm 0 0 m -0.78 -0.18 l S 1 0 0 1 -1.26 -0.3 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.72 -0.18 cm 0 0 m -0.18 -0.12 l S 1 0 0 1 -0.72 -0.24 cm 0 0 m -0.78 -0.24 l S 1 0 0 1 -1.26 -0.42 cm 0 0 m -0.18 -0.06 l -0.24 -0.06 l S 1 0 0 1 -0.72 -0.36 cm 0 0 m -0.18 -0.06 l S 1 0 0 1 -0.72 -0.36 cm 0 0 m -0.78 -0.36 l S 1 0 0 1 -1.26 -0.6 cm 0 0 m -0.12 -0.06 l -0.18 -0.12 l S 1 0 0 1 -0.72 -0.54 cm 0 0 m -0.18 -0.18 l S 1 0 0 1 -0.72 -0.66 cm 0 0 m -0.78 -0.66 l S 1 0 0 1 -1.26 -1.08 cm 0 0 m -0.06 -0.06 l -0.18 -0.18 l S 1 0 0 1 -0.54 -0.72 cm 0 0 m -0.18 -0.18 l S 1 0 0 1 -0.54 -0.72 cm 0 0 m -0.54 -0.72 l S 1 0 0 1 -0.9 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.18 -0.24 l S 1 0 0 1 -0.48 -0.78 cm 0 0 m -0.36 -0.72 l S 1 0 0 1 -0.66 -1.2 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.36 -0.78 cm 0 0 m -0.42 -0.72 l S 1 0 0 1 -0.66 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.36 -0.72 cm 0 0 m -0.06 -0.12 l -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.3 -0.78 l S 1 0 0 1 -0.48 -1.26 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.12 -0.18 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.3 -0.78 l S 1 0 0 1 -0.54 -1.26 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.12 -0.18 l S 1 0 0 1 -0.36 -0.72 cm 0 0 m -0.24 -0.54 l -0.24 -0.72 l S 1 0 0 1 -0.48 -1.26 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.24 -0.66 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.78 cm 0 0 m -0.3 -0.72 l S 1 0 0 1 -0.42 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.78 cm 0 0 m -0.24 -0.72 l S 1 0 0 1 -0.42 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.24 -0.78 l S 1 0 0 1 -0.42 -1.26 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.24 -0.78 l S 1 0 0 1 -0.42 -1.26 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.24 -0.72 l S 1 0 0 1 -0.42 -1.26 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.3 -0.66 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.78 cm 0 0 m -0.24 -0.72 l S 1 0 0 1 -0.42 -1.2 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.3 -0.78 cm 0 0 m -0.24 -0.72 l S 1 0 0 1 -0.36 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.24 -0.78 l S 1 0 0 1 -0.42 -1.26 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.24 -0.78 l S 1 0 0 1 -0.48 -1.26 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.24 -0.72 cm 0 0 m -0.12 -0.18 l S 1 0 0 1 -0.3 -0.72 cm 0 0 m -0.3 -0.78 l S 1 0 0 1 -0.54 -1.26 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -0.3 -0.66 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.3 -0.78 cm 0 0 m -0.06 -0.18 l -0.3 -0.72 l S 1 0 0 1 -0.54 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.36 -0.72 cm 0 0 m -0.06 -0.24 l S 1 0 0 1 -0.36 -0.78 cm 0 0 m -0.36 -0.72 l S 1 0 0 1 -0.6 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.36 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.36 -0.72 cm 0 0 m -0.12 -0.24 l -0.48 -0.78 l S 1 0 0 1 -0.78 -1.26 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.54 -0.78 l S 1 0 0 1 -0.84 -1.26 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.6 -0.72 cm 0 0 m -0.24 -0.18 l S 1 0 0 1 -0.78 -0.72 cm 0 0 m -0.72 -0.72 l S 1 0 0 1 -1.2 -1.2 cm 0 0 m -0.18 -0.18 l -0.24 -0.24 l S 1 0 0 1 -0.72 -0.48 cm 0 0 m -0.24 -0.18 l S 1 0 0 1 -0.78 -0.42 cm 0 0 m -0.72 -0.42 l S 1 0 0 1 -1.2 -0.72 cm 0 0 m -0.12 0 l -0.24 -0.06 l S 1 0 0 1 -0.72 -0.12 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.78 -0.12 cm 0 0 m -0.72 -0.06 l S 1 0 0 1 -1.2 -0.18 cm 0 0 m -0.06 0 l -0.24 0.06 l S 1 0 0 1 -0.72 0.18 cm 0 0 m -0.24 0.06 l S 1 0 0 1 -0.78 0.24 cm 0 0 m -0.72 0.18 l S 1 0 0 1 -1.2 0.36 cm 0 0 m 0 0 l -0.24 0.12 l S 1 0 0 1 -0.72 0.36 cm 0 0 m -0.24 0.12 l S 1 0 0 1 -0.72 0.42 cm 0 0 m -0.78 0.42 l S 1 0 0 1 -1.26 0.66 cm 0 0 m -0.24 0.12 l S 1 0 0 1 -0.72 0.42 cm 0 0 m -0.24 0.12 l S 1 0 0 1 -0.72 0.42 cm 0 0 m -0.78 0.42 l S 1 0 0 1 -1.26 0.72 cm 0 0 m -0.24 0.06 l S 1 0 0 1 -0.72 0.3 cm 0 0 m -0.24 0.06 l S 1 0 0 1 -0.72 0.3 cm 0 0 m -0.78 0.36 l S 1 0 0 1 -1.26 0.6 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 0.12 cm 0 0 m -0.24 0.06 l S 1 0 0 1 -0.72 0.18 cm 0 0 m -0.78 0.18 l S 1 0 0 1 -1.26 0.24 cm 0 0 m -0.24 0.06 l S 1 0 0 1 -0.72 0.12 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.72 0 cm 0 0 m -0.78 0.12 l S 1 0 0 1 -1.26 0.06 cm 0 0 m -0.24 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.18 0 l S 1 0 0 1 -0.72 -0.06 cm 0 0 m -0.78 -0.06 l S 1 0 0 1 -1.26 -0.12 cm 0 0 m -0.18 -0.06 l S 1 0 0 1 -0.72 -0.18 cm 0 0 m -0.18 -0.06 l S 1 0 0 1 -0.72 -0.18 cm 0 0 m -0.78 -0.12 l S 1 0 0 1 -1.26 -0.3 cm 0 0 m -0.18 -0.12 l S 1 0 0 1 -0.66 -0.3 cm 0 0 m -0.24 -0.06 l S 1 0 0 1 -0.78 -0.3 cm 0 0 m -0.72 -0.24 l S 1 0 0 1 -1.26 -0.54 cm 0 0 m -0.18 -0.12 l S 1 0 0 1 -0.66 -0.36 cm 0 0 m -0.24 -0.18 l S 1 0 0 1 -0.78 -0.48 cm 0 0 m -0.72 -0.42 l S 1 0 0 1 -1.26 -0.84 cm 0 0 m -0.18 -0.18 l S 1 0 0 1 -0.66 -0.54 cm 0 0 m -0.24 -0.18 l S 1 0 0 1 -0.78 -0.66 cm 0 0 m -0.66 -0.48 l -0.72 -0.6 l S 1 0 0 1 -1.2 -1.08 cm 0 0 m -0.18 -0.18 l S 1 0 0 1 -0.6 -0.66 cm 0 0 m -0.24 -0.24 l S 1 0 0 1 -0.72 -0.78 cm 0 0 m -0.66 -0.72 l S 1 0 0 1 -1.08 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.18 -0.24 l S 1 0 0 1 -0.54 -0.78 cm 0 0 m -0.54 -0.72 l S 1 0 0 1 -0.9 -1.2 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.48 -0.78 l S 1 0 0 1 -0.78 -1.26 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.42 -0.72 cm 0 0 m -0.12 -0.24 l S 1 0 0 1 -0.48 -0.72 cm 0 0 m -0.42 -0.78 l S 1 0 0 1 -377.64 -622.74 cm BT /TT0 1 Tf 0 Tc 5.1471 0 0 5.1471 432.78 720.36 Tm ( )Tj -0.00169 Tc -0.0007 Tw 0 6.3169 -6.3169 0 322.74 635.7 Tm [(Cu)-6 (r)-10.6 (r)-1.1 (e)-5.9 (n)-15.5 (t / )-9.5 (m)-4.5 (A)]TJ 0.0054 Tc -0.0078 Tw 6.3169 0 0 6.3169 383.16 570.42 Tm [(P)7.5 (o)-8.3 (t)7.8 (e)1.1 (n)-8.3 (t)7.8 (ial /)7.8 ( )-9.5 (V)7.5 ( )]TJ /TT2 1 Tf 0.0024 Tc 0 Tw [0.3 (ve)-11.4 (rsu)-11.3 (s)]TJ /TT0 1 Tf -0.0027 Tc 0.00031 Tw [-0.4 ( A)-10.1 (g)-6.9 (/A)-10.1 (g)-6.9 (C)-11.9 (l/)-9.8 (KC)-11.9 (l)]TJ 0.00031 Tc 0 Tw 3.7767 0 0 3.7767 475.2 567.96 Tm [(\(s)-8.1 (at)8.1 (.)-7.8 (\))]TJ ET 1 0 0 1 462.78 633.36 cm 0 0 m 12.78 0 l S 1 0 0 1 -462.78 -633.36 cm BT /TT0 1 Tf 0.0047 Tc 0.0009 Tw 5.7152 0 0 5.7152 475.56 631.44 Tm [( fi)6.4 (rst )10.5 (sca)-6 (n)]TJ ET 1 0 0 1 462.78 626.4 cm 0 0 m 0.78 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.8 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.84 0 l S 1 0 0 1 1.8 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.74 0 cm 0 0 m 0.42 0 l S 1 0 0 1 -475.08 -626.4 cm BT /TT0 1 Tf 0.00169 Tc 0.00391 Tw 5.7152 0 0 5.7152 475.56 624.42 Tm ( second scan)Tj ET 1 0 0 1 462.78 619.38 cm 0 0 m 0.18 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.18 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.18 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.24 0 l S 1 0 0 1 1.14 0 cm 0 0 m 0.18 0 l S 1 0 0 1 1.08 0 cm 0 0 m 0.18 0 l S 1 0 0 1 -474.72 -619.38 cm BT /TT0 1 Tf 0.00481 Tc 0.00079 Tw 5.7152 0 0 5.7152 475.56 617.46 Tm [( th)4.5 (i)6.5 (r)1.9 (d)4.5 ( sca)4.5 (n)]TJ ET 1 0 0 1 462.78 612.42 cm 0 0 m 0.96 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.18 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.78 0 cm 0 0 m 1.02 0 l S 1 0 0 1 1.5 0 cm 0 0 m 0 0 l S 1 0 0 1 -475.5 -612.42 cm BT /TT0 1 Tf 0.0043 Tc 0.0013 Tw 5.7152 0 0 5.7152 475.56 610.5 Tm [( fo)4 (rt)9.2 (h)4 ( sca)4 (n)]TJ ET 1 0 0 1 462.78 605.46 cm 0 0 m 0.72 0 l S 1 0 0 1 1.2 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0.78 0 l S 1 0 0 1 1.26 0 cm 0 0 m 0.24 0 l S 1 0 0 1 0.72 0 cm 0 0 m 0 0 l S 1 0 0 1 -475.5 -605.46 cm BT /TT0 1 Tf 0.005 Tc 0.0006 Tw 5.7152 0 0 5.7152 475.56 603.48 Tm [( fi)6.7 (fth)4.7 ( )10.5 (sca)-5.7 (n)]TJ /TT1 1 Tf -0.01131 Tc 0 Tw 6.3169 0 0 6.3169 359.58 695.4 Tm (\(b\))Tj /TT3 1 Tf 0 Tc 12 0 0 12 412.98 542.88 Tm ( )Tj /TT4 1 Tf 0.0004 Tc 0.43961 Tw -26.915 -1.465 Td (Figure 4.)Tj /TT3 1 Tf 0 Tc 0.411 Tw 4.275 0 Td ( Subsequent scans of \(a\) Cu/BDD )Tj 0.0004 Tc 0.40961 Tw 16.24 0 Td [(and \(b\) Cu/BDUND electrodes for)-6.6 ( )410 ( )]TJ 0.0006 Tc 0.1244 Tw -20.515 -1.15 Td [(0.001 m)8.4 (o)0.6 (l L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 151.92 517.02 Tm (-1)Tj 0.00031 Tc 0.1201 Tw 12 0 0 12 158.58 511.5 Tm ( BR buffer and for nitrate reduction in solution of 0.01 mol L)Tj -0.0022 Tc 0 Tw 7.98 0 0 7.98 469.62 517.02 Tm (-1)Tj 0.00281 Tc 0.1172 Tw 12 0 0 12 476.28 511.5 Tm ( KNO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 506.7599 510 Tm (3)Tj 0.00101 Tc 0.119 Tw 12 0 0 12 510.78 511.5 Tm ( + )Tj 0.0006 Tc 0.00191 Tw -35.065 -1.15 Td [(0.001 m)8.4 (o)0.6 (l L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 148.98 503.22 Tm (-1)Tj -0.00031 Tc 0.00031 Tw 12 0 0 12 155.64 497.7 Tm ( BR buffer. )Tj 0 Tc 0 Tw -3.98 -1.15 Td ( )Tj 0 -1.15 TD ( )Tj 0.00031 Tc 0.1138 Tw T* (In the subsequent scans of nitrate reduc)Tj 0.1134 Tw 16.47 0 Td (tion, the cathodic peak cu)Tj 0.1122 Tw 10.705 0 Td (rrent decreased in )Tj 0.0006 Tc 0.09039 Tw -28.665 -1.15 Td [(the third m)8.4 (easurem)8.4 (ent for Cu/BDUND fil)-6.6 (m)8.4 (, )]TJ 0.0004 Tc 0.0896 Tw 18.57 0 Td (indicating that all Cu photoeletrodeposited )Tj 0.0152 Tw -18.57 -1.15 Td [(cam)8.1 (e out of the BDUND surface. It is noted th)]TJ 0.0007 Tc 0.013 Tw 18.795 0 Td [(at fro)-4.3 (m)8.5 ( the third sca)]TJ -0.0002 Tc 0.0135 Tw 8.115 0 Td (n, the nitrate reduction )Tj -0.00011 Tc 0.0293 Tw -26.91 -1.15 Td [(response was the sam)7.7 (e)-1.3 ( for the as-grown BD)]TJ 0.0005 Tc 0.02699 Tw 17.775 0 Td (UND electrode. Convers)Tj 0.0006 Tc 0.02769 Tw 9.975 0 Td [(ely, for the Cu/B)7.6 (DD )]TJ 0.00031 Tc 0.31219 Tw -27.75 -1.15 Td (electrode the reproducibility )Tj 0.00011 Tc 0.31149 Tw 12.525 0 Td (was evident, indicating that)Tj 0.00031 Tc 0.3134 Tw 11.935 0 Td [( the copper particles were)-5.9 ( )]TJ 0.00079 Tc 0.07581 Tw -24.46 -1.15 Td [(consolid)5.8 (ated)5.8 ( in the electrode )]TJ -0.0005 Tc 0.08051 Tw [0.4 (surface. This behavior can be )]TJ -0.00031 Tc 0.07899 Tw 24.415 0 Td (explained by the Cu particle )Tj 0.0006 Tc 0.04359 Tw -24.415 -1.15 Td [(deposition o)5.6 (n)0.6 ( the diam)8.4 (ond faces while, for th)]TJ 0.0004 Tc 0.0446 Tw 18.42 0 Td [(e BDUND, a suitab)5.4 (l)-1.8 (e de)]TJ 0.00079 Tc 0.0425 Tw 9.93 0 Td [(p)5.8 (o)0.8 (sit on its)5 ( s)5 (u)0.8 (rface )]TJ -0.00011 Tc 0.00011 Tw -28.35 -1.15 Td (was not obtained in order to assure)Tj 0 Tc 0 Tw 13.945 0 Td ( the Cu particles consolidation. )Tj 0.0002 Tc 0.03481 Tw -12.455 -1.15 Td [(This study showed that the copper photoe)1.8 (lectrodeposition process on sem)8 (i)-2 (conducting )]TJ 0.0006 Tc 0.0681 Tw -1.49 -1.15 Td [(diam)8.4 (ond surface can be a good alternative for th)]TJ 0.0002 Tc 0.0714 Tw 19.88 0 Td [(e preparatio)5.2 (n of m)8 (odi)]TJ 0.0006 Tc 0.06689 Tw 8.84 0 Td (fied electrode. By )Tj 0.00031 Tc 0.1747 Tw -28.72 -1.15 Td [(applying U)7.5 (V)2.5 ( irradiation, the copper photoele)]TJ -0.0002 Tc 0.1752 Tw 18.87 0 Td (ctrodeposition and its )Tj 0 Tc 0.17 Tw 9.38 0 Td (consolidation were )Tj 0.00031 Tc -0.00031 Tw -28.25 -1.15 Td [(more efficient on the B)7.3 (DD than those on the B)7.3 (DUND electrode.)5.3 ( )]TJ 0 Tc 0 Tw T* ( )Tj /TT4 1 Tf 0.00121 Tc 14.08 -1.16 Td [(A)3.4 (cknow)8.4 (ledgments)5.4 ( )]TJ /TT3 1 Tf 0 Tc -14.08 -1.14 Td ( )Tj ET 1 g 107.88 246.6 414.12 13.98 re f BT 0 g /TT3 1 Tf 0.0004 Tc 0.01871 Tw 12 0 0 12 107.88 249.3 Tm (The authors are very grateful to FA)Tj 0.0002 Tc 0.01981 Tw 14.285 0 Td (PESP \(Process 2010/05391-0\), CAPES and CNPq )Tj ET 1 g 90 232.8 131.58 13.98 re f BT 0 g /TT3 1 Tf 0.00031 Tc 0.2047 Tw 12 0 0 12 90 235.5 Tm [(for the financial support. Special thanks to Eduardo Saito and Fernando \ Al)-6.9 (m)8.1 (e)-0.9 (ida de )]TJ -0.0014 Tw T* [(Souza for providing the diam)8.2 (ond samples. )]TJ 0 Tc 0 Tw T* ( )Tj /TT4 1 Tf 0.0007 Tc -0.00571 Tw 15.665 -1.16 Td (References )Tj /TT3 1 Tf 0 Tc 0 Tw -15.665 -1.14 Td ( )Tj -0.00011 Tc 0.0101 Tw 1.49 -1.15 Td (1. S. Ghafari, M. Hasan, M.K. Aroua, )Tj /TT5 1 Tf 0.0002 Tc 0.0098 Tw [-0.2 (Bioresource Technology,)]TJ /TT3 1 Tf 0 Tc 0 Tw 25.49 0 Td ( )Tj /TT4 1 Tf 0.26 0 Td (99)Tj /TT3 1 Tf -0.0005 Tc 0.0105 Tw (, 3965-3974 \(2008\). )Tj 0.0002 Tc 0.1756 Tw -25.75 -1.15 Td (2. M. Li, C. Feng, Z. Zha)Tj 0.17599 Tw [-0.5 (ng, S. Yang, N. Sugiura, )]TJ /TT5 1 Tf 0.00011 Tc 0.1749 Tw (Bioresource Technology)Tj /TT3 1 Tf 0 Tc 0 Tw 32.09 0 Td (, )Tj /TT4 1 Tf 0.675 0 Td (101)Tj /TT3 1 Tf -0.005 Tc (, )Tj 0.00011 Tc -0.00011 Tw -32.755 -1.15 Td (6553-6557 \(2010\). )Tj ET 1 g 106.38 122.34 417.12 13.8 re f BT 0 g /TT3 1 Tf 0.0002 Tc 0.0556 Tw 12 0 0 12 107.88 125.1 Tm (3. A.N. Ndao, F. Zenia, A. Deneuv)Tj 0.0005 Tc 0.0545 Tw [0.2 (ille, M. Berna)4.3 (r)-1.5 (d, C. L\351vy-Cl\351m)8.3 (ent, )]TJ /TT5 1 Tf -0.0006 Tc 0.06059 Tw 28.975 0 Td [(Di)-7.8 (amond and )]TJ ET 1 g 106.38 108.54 417.12 13.8 re f BT 0 g /TT5 1 Tf 0.0007 Tc -0.00571 Tw 12 0 0 12 108 111.3 Tm (Related Materials,)Tj /TT3 1 Tf 0 Tc 0 Tw 7.45 0 Td ( )Tj /TT4 1 Tf (9)Tj /TT3 1 Tf -0.0002 Tc 0.0002 Tw (, 1175-1180 \(2000\). )Tj ET 1 g 106.38 94.74 417.12 13.8 re f BT 0 g /TT3 1 Tf -0.00011 Tc 0.4659 Tw 12 0 0 12 107.88 97.5001 Tm [(4. C. L\351vy-Cl\351m)7.7 (e)-1.3 (nt, N.A. Nda)-6.3 (o, A. Ka)]TJ 0.00031 Tc 0.46471 Tw 18.485 0 Td (tty, M. Bernard, A. Deneuville, C. )Tj ET 1 g 106.38 80.94 417.12 13.8 re f BT 0 g /TT3 1 Tf 0.0006 Tc -0.0006 Tw 12 0 0 12 108 83.7 Tm [(Com)8.4 (n)0.6 (inellis)4.8 (, A. Fujishim)8.4 (a)-0.6 (, )]TJ /TT5 1 Tf 0.00031 Tc -0.00031 Tw 11.11 0 Td (Diamond and Related Materials)Tj /TT3 1 Tf -0.005 Tc 0 Tw 12.925 0 Td (, )Tj /TT4 1 Tf 0 Tc 0.495 0 Td (12)Tj /TT3 1 Tf -0.0002 Tc 0.0002 Tw (, 606-612 \(2003\). )Tj ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 298.5 12 Td (182)Tj ET Q BT /GS1 gs /T1_1 1 Tf 0 Tc 0 Tw 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_1 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_1 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 34 0 obj <> endobj 21 0 obj <> endobj 33 0 obj <> endobj 31 0 obj <> endobj 20 0 obj <> endobj 32 0 obj <> endobj 94 0 obj <> endobj 101 0 obj <> endobj 102 0 obj <> endobj 103 0 obj <> endobj 89 0 obj [104 0 R 105 0 R] endobj 90 0 obj <>stream BT /GS0 gs /TT0 1 Tf 0.0007 Tc 0.04359 Tw 12 0 0 12 107.88 726.84 Tm [(In the case of the BDUND electrod)5.7 (e)-0.5 (, the possi)]TJ 0.00121 Tc 0.04289 Tw 18.955 0 Td [(b)6.2 (l)-1 (e reac)5 (tions that occu)6.2 (r in)6.2 ( this process )]TJ 0.00031 Tc 0.08971 Tw -20.445 -1.15 Td [(should be analyzing considering its a)-5.9 (m)8.1 (or)]TJ 0.0005 Tc 0.08949 Tw 16.875 0 Td [(phous se)-5.7 (m)8.3 (i)-1.7 (conductor character. Due to the sp)]TJ 0 Tc 0 Tw 7.98 0 0 7.98 518.0399 718.56 Tm (2)Tj 12 0 0 12 521.9999 713.04 Tm ( )Tj 0.0005 Tc 0.2245 Tw -36 -1.15 Td (bonds presence, this disorder reduces th)Tj 0.00011 Tc 0.22549 Tw 17.08 0 Td [(e BDUND band gap by a b)-4.9 (a)-1 (nd tailing with )]TJ 0.0005 Tc 0.0985 Tw -17.08 -1.15 Td [(additional states, which im)8.3 (proves its conductivit)]TJ 0.0006 Tc 0.0994 Tw 19.83 0 Td (y \(15\). In this case,)Tj 0.0002 Tc 0.09641 Tw [0.1 ( the electron excess )]TJ 0.0004 Tc 0.05791 Tw -19.83 -1.15 Td (by the photoprocess also)Tj 0 Tc 0.06 Tw 10.035 0 Td [( occurs.)5 ( Nonetheless, fo)5 (r the )]TJ -0.0005 Tc 0.0605 Tw 11.93 0 Td (BDUND a significa)Tj -0.0004 Tc 8.06 0 Td (nt contribution )Tj 0.0004 Tc 0.0779 Tw -30.025 -1.23 Td (to its conductivity is)Tj -0.0009 Tc 0.0809 Tw 8.38 0 Td ( the effect of sp)Tj 0 Tc 0 Tw 7.98 0 0 7.98 268.92 662.4 Tm (2)Tj 0.00011 Tc 0.0786 Tw 12 0 0 12 272.94 656.88 Tm ( bonding indicated by the )Tj /T1_0 1 Tf -0.004 Tc 0 Tw 10.81 0 Td (\004 )Tj /TT0 1 Tf 0.00031 Tc 0.795 0 Td (and )Tj /T1_0 1 Tf 0.0005 Tc 1.775 0 Td (\004\005 )Tj /TT0 1 Tf 0.00031 Tc 0.07719 Tw 1.3 0 Td (bands. For this )Tj 0.0002 Tc 0.1239 Tw -29.925 -1.145 Td [(reason, we believe that the recom)8 (b)0.2 (ination fo)]TJ 0.0007 Tc 0.1236 Tw [-0.1 (r BDUND is faster than that for the BDD )]TJ 0.0004 Tc 0.0629 Tw 0 -1.15 TD [(electrode reducing th)5.4 (e p)5.4 (hotoeff)]TJ 0.0006 Tc 0.06371 Tw 12.71 0 Td [(ect contribu)5.6 (tion to of additio)5.6 (nal electron)5.6 (s)-0.2 ( involved)5.6 ( in the )]TJ 0.0004 Tc 0.2542 Tw -12.71 -1.15 Td (Cu deposition. This behavior led to the lowest density of Cu deposits on\ BDUND )Tj 0.0006 Tc 0 Tw T* [(surface.)5.6 ( )]TJ 0.00079 Tc 0.0083 Tw 1.49 -1.15 Td [(These m)8.6 (odified film)8.6 (s were used to ev)5.8 (aluate)]TJ 0.0007 Tc 0.0076 Tw 17.495 0 Td [( their perform)8.5 (a)-0.5 (nce to )]TJ -0.0004 Tc 0.01041 Tw 8.7 0 Td (the nitrate reduction. )Tj 0.0004 Tc 0.04871 Tw -27.685 -1.15 Td [(Figure 3 presents linear sweep voltamogram)8.2 (s in)]TJ 0.0006 Tc 0.05009 Tw 19.46 0 Td [( the pres)4.8 (ence of nitrate for as-g)5.6 (rown and)5.6 ( )]TJ 0.0011 Tc 0.0139 Tw -19.46 -1.15 Td [(Cu/diam)8.9 (ond f)4.1 (ilm)8.9 (s. For both ele)4.9 (c)-0.1 (trod)6.1 (es, the c)4.9 (a)]TJ 0.0004 Tc 0.0137 Tw 18.425 0 Td [(tho)5.4 (d)0.4 (ic currents for buffer BR are associated)5.4 ( )]TJ 0.0005 Tc 0.2587 Tw -18.425 -1.15 Td (to water reduction. It is possible to obs)Tj 0.0006 Tc 0.25771 Tw 17.33 0 Td [(erve that Cu deposited on diam)8.4 (ond surface )]TJ 0.0004 Tc 0.0329 Tw -17.33 -1.15 Td (catalyse the electroreduction of )Tj 0.0006 Tc 0.03439 Tw 12.915 0 Td [(nitrate for both electrod)5.6 (e)-0.6 (s. The nitrate electroreductio)5.6 (n)0.6 ( is )]TJ 0 Tc 0.16499 Tw -12.915 -1.15 Td (a very complex process. Several products )Tj -0.00011 Tc 0.16341 Tw 17.84 0 Td (are possible depending on)Tj 0.00011 Tc 0.1624 Tw 10.9 0 Td [( the experim)7.9 (e)-1.1 (ntal )]TJ -0.00011 Tc 0.1842 Tw -28.74 -1.15 Td (conditions such as pH and applied potential.)Tj -0.0009 Tc 0.1859 Tw 18.795 0 Td ( In this work, only one cathodic peak is )Tj 0 Tc 0.295 Tw -18.795 -1.15 Td [(observed around -1.25 V for bot)-7.2 (h as-grown di)]TJ 0.00031 Tc 0.2959 Tw 20.46 0 Td [(am)8.1 (ond film)8.1 (s, suggesting that nitrate )]TJ 0.0007 Tc 0.0943 Tw -20.46 -1.15 Td [(reduction to a)-5.5 (m)3.5 (m)8.5 (onia is taking place at this )]TJ 0.0004 Tc 0.0946 Tw 18.495 0 Td [(potentia)4.3 (l. The effect of)]TJ 0.0006 Tc 0.0956 Tw 9.445 0 Td ( Cu deposits on the )Tj 0.00011 Tc 0.0549 Tw -27.94 -1.15 Td [(diam)7.9 (ond surface was m)7.9 (o)-4.9 (re pronounced in the BDD than that for the BD)7.3 (UND due to the )]TJ 0.0006 Tc -0.0013 Tw T* [(greatest am)8.4 (ount of Cu on its su)5.6 (rface. )]TJ /TT1 1 Tf 0.00169 Tc 0 Tw 4.9366 0 0 4.9366 130.98 292.0201 Tm [(-)-5.6 (1)10.9 (.8)-2213.3 (-)6.5 (1)-1.2 (.)12.1 (6)-2225.4 (-)-5.6 (1)10.9 (.4)-2213.3 (-)6.5 (1)10.9 (.2)-2213.3 (-)-5.6 (1)10.9 (.0)-2213.3 (-)6.5 (0)10.9 (.8)-2225.4 (-)6.5 (0)-1.2 (.)12.1 (6)-2213.3 (-)-5.6 (0)10.9 (.4)]TJ 0.00729 Tc -3.9136 1.0574 Td [(-0)16.5 (.)5.6 (1)16.5 (6)]TJ 0 2.8197 TD [(-0)16.5 (.)5.6 (1)16.5 (4)]TJ T* [(-0)16.5 (.)5.6 (1)16.5 (2)]TJ 0 2.8076 TD [(-0)16.5 (.)5.6 (1)16.5 (0)]TJ T* [(-0)16.5 (.)5.6 (0)16.5 (8)]TJ 0 2.8197 TD [(-0)16.5 (.)5.6 (0)16.5 (6)]TJ 0 2.8076 TD [(-0)16.5 (.)5.6 (0)16.5 (4)]TJ T* [(-0)16.5 (.)5.6 (0)16.5 (2)]TJ -0.0092 Tc 0.3403 2.8197 Td [(0.)-10.9 (00)]TJ 0 2.8197 TD [(0.)-10.9 (02)]TJ ET 1 0 0 1 125.52 298.5 cm 0.463 w 1 j 1 J 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.72 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.66 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.66 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.72 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.66 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.72 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.72 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.46 l S 1 0 0 1 9.66 0 cm 0 0 m 0 1.26 l S 1 0 0 1 -155.34 0 cm 0 0 m 155.34 0 l S 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.9 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.9 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.9 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.9 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.46 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.9 cm 0 0 m 2.46 0 l S 1 0 0 1 0 -124.98 cm 0 0 m 0 124.98 l 0 124.98 l S 1 0 0 1 9.72 124.98 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.66 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.66 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.66 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.66 0 cm 0 0 m 0 0 l S 1 0 0 1 -155.34 0 cm 0 0 m 155.34 0 l S 1 0 0 1 155.34 -124.98 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.9 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.9 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.9 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.9 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.9 cm 0 0 m 0 0 l S 1 0 0 1 0 -124.98 cm 0 0 m 0 124.98 l S 1 0 0 1 -9.66 111.06 cm 0.321 w 0 0 m -1.44 0 l S 1 0 0 1 -4.74 0 cm 0 0 m -1.44 0 l S 1 0 0 1 -4.74 0 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.12 cm 0 0 m -1.44 0 l S 1 0 0 1 -4.74 0 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.12 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.12 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.68 -0.12 cm 0 0 m -1.44 0 l S 1 0 0 1 -4.74 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.18 cm 0 0 m -1.38 -0.06 l S 1 0 0 1 -4.68 -0.24 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.8 -0.6 cm 0 0 m -1.44 -0.3 l S 1 0 0 1 -4.74 -1.2 cm 0 0 m -1.38 -0.6 l S 1 0 0 1 -4.68 -2.16 cm 0 0 m -1.44 -0.54 l S 1 0 0 1 -4.8 -1.98 cm 0 0 m -1.44 -0.9 l S 1 0 0 1 -4.74 -3.3 cm 0 0 m -1.38 -1.2 l S 1 0 0 1 -4.68 -4.2 cm 0 0 m -1.44 -1.38 l S 1 0 0 1 -4.8 -4.8 cm 0 0 m -1.26 -1.44 l S 1 0 0 1 -4.68 -5.4 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 -4.8 -5.76 cm 0 0 m -1.14 -1.44 l S 1 0 0 1 -4.74 -6 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.28 -3.06 cm 0 0 m 0 0 l S 1 0 0 1 -2.4 -3.06 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.34 -3.06 cm 0 0 m -0.06 -0.06 l S 1 0 0 1 -2.46 -3.3 cm 0 0 m -1.08 -1.38 l S 1 0 0 1 -2.28 -3 cm 0 0 m -0.06 -0.06 l S 1 0 0 1 -2.46 -3.24 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.28 -3.06 cm 0 0 m 0 -0.06 l S 1 0 0 1 116.1 58.14 cm 0 0 m -2.4 0 l -4.74 -0.06 l -9.48 -0.06 l -11.88 -0.12 l -18.96 -0.12 l -21.36 -0.18 l -23.7 -0.12 l -26.1 -0.18 l -28.44 -0.24 l -33.24 -0.36 l -35.58 -0.48 l -37.92 -0.54 l -40.32 -0.72 l -42.66 -1.02 l -45.06 -1.38 l -47.46 -1.92 l -49.8 -2.76 l -52.14 -3.96 l -54.54 -5.88 l -56.94 -8.7 l -59.28 -12.84 l -61.68 -18.24 l -64.02 -24.78 l -66.36 -31.92 l -68.76 -39.12 l -71.16 -45.96 l -73.5 -51.72 l -75.9 -56.46 l -78.24 -60.12 l -80.58 -62.64 l -82.98 -63.72 l -85.38 -63.54 l -87.72 -62.04 l -90.06 -60 l -92.46 -57.9 l -94.86 -56.04 l -97.2 -54.6 l -99.6 -53.7 l -101.94 -53.16 l -104.28 -53.1 l -106.68 -53.04 l -109.08 -53.1 l -111.42 -53.16 l -113.82 -53.52 l -116.16 -54.18 l -118.56 -55.2 l S 1 0 0 1 0 -0.48 cm 0.5 G 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.18 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.24 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.24 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.36 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.74 -0.6 cm 0 0 m -1.44 -0.24 l S 1 0 0 1 -4.74 -0.84 cm 0 0 m -1.44 -0.48 l S 1 0 0 1 -4.8 -1.56 cm 0 0 m -1.44 -0.6 l S 1 0 0 1 -4.68 -2.28 cm 0 0 m -1.44 -0.9 l S 1 0 0 1 -4.74 -3.18 cm 0 0 m -1.44 -1.2 l S 1 0 0 1 -4.8 -4.02 cm 0 0 m -1.38 -1.32 l S 1 0 0 1 -4.68 -4.62 cm 0 0 m -1.38 -1.44 l S 1 0 0 1 -4.8 -5.04 cm 0 0 m -1.26 -1.44 l S 1 0 0 1 -4.74 -5.58 cm 0 0 m -1.14 -1.44 l S 1 0 0 1 -4.68 -6 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.34 -3 cm 0 0 m -0.06 -0.12 l S 1 0 0 1 -2.46 -3.36 cm 0 0 m -1.02 -1.44 l S 1 0 0 1 -2.16 -3.06 cm 0 0 m -0.18 -0.18 l S 1 0 0 1 -2.58 -3.54 cm 0 0 m -0.96 -1.44 l S 1 0 0 1 -2.04 -3.06 cm 0 0 m -0.24 -0.36 l S 1 0 0 1 -2.64 -3.84 cm 0 0 m -1.02 -1.44 l S 1 0 0 1 -2.16 -3.06 cm 0 0 m -0.24 -0.3 l S 1 0 0 1 -2.64 -3.84 cm 0 0 m -0.96 -1.38 l S 1 0 0 1 -2.04 -3 cm 0 0 m -0.24 -0.36 l S 1 0 0 1 -2.64 -3.78 cm 0 0 m -1.02 -1.44 l S 1 0 0 1 -2.16 -3.06 cm 0 0 m -0.18 -0.24 l S 1 0 0 1 -2.64 -3.48 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -4.74 -6 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 -4.68 -5.4 cm 0 0 m -1.44 -1.44 l S 1 0 0 1 -4.8 -4.68 cm 0 0 m -1.44 -1.26 l S 1 0 0 1 -4.74 -3.78 cm 0 0 m -1.38 -0.84 l S 1 0 0 1 113.82 95.1 cm 0 0 m -2.4 -0.06 l -4.74 -0.06 l -7.14 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[(Curren)3.7 (t)2.6 ( / )-9.9 (mA)]TJ -0.002 Tc 0.0015 Tw 6.0586 0 0 6.0586 155.1 282.2401 Tm [(Po)-10.3 (te)-10.3 (nti)-7.6 (a)-10.3 (l / V)-8.4 ( )]TJ /TT3 1 Tf 0.00591 Tc 0 Tw 5.6944 0 Td [(ve)7.5 (rsus)]TJ /TT1 1 Tf -0.0023 Tc 0.0018 Tw 2.971 0 Td [( Ag)-10.6 (/Ag)-10.6 (C)-3.1 (l)-7.9 (/)-1.8 (K)-8.7 (C)-3.1 (l)]TJ -0.0024 Tc 0 Tw 3.6223 0 0 3.6223 243.12 279.8401 Tm [(\(sa)-9.4 (t)-6.2 (.)10.4 (\))]TJ ET 1 0 0 1 191.82 329.7 cm 0 G 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 -204 -329.7 cm BT /TT1 1 Tf 0.0009 Tc 0.00591 Tw 5.4815 0 0 5.4815 205.74 327.84 Tm [( BD)11.6 (D_Bu)9.8 (f)-5.9 (f)-5.9 (e)9.8 (r)-5.4 ( B)11.1 (R)0.6 ( )]TJ ET 1 0 0 1 191.82 322.98 cm 0 0 m 13.92 0 l S 1 0 0 1 -191.82 -322.98 cm BT /TT1 1 Tf 0.0067 Tc 0.00011 Tw 5.4815 0 0 5.4815 205.74 321.12 Tm [( B)6 (D)17.4 (D)6.4 (_)4.6 (B)6 (u)15.6 (ffe)15.6 (r B)16.9 (R)6.4 ( +)10.6 ( n)15.6 (i)-1 (t)10.9 (r)0.4 (a)15.6 (t)-0.1 (e)]TJ ET 1 0 0 1 191.82 316.26 cm 0.5 G 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 -204 -316.26 cm BT /TT1 1 Tf 0.0058 Tc 0.00101 Tw 5.4815 0 0 5.4815 205.74 314.4 Tm [( C)16.5 (u)3.7 (/B)5.1 (D)16.5 (D)5.5 (_B)5.1 (u)14.7 (ffe)14.7 (r B)16 (R)]TJ ET 1 0 0 1 191.82 309.6 cm 0 0 m 13.92 0 l S 1 0 0 1 -191.82 -309.6 cm BT /TT1 1 Tf 0.00591 Tc 0.0009 Tw 5.4815 0 0 5.4815 205.74 307.74 Tm [( C)16.6 (u)3.8 (/B)5.2 (D)16.6 (D)5.6 (_B)5.2 (u)14.8 (ffe)14.8 (r B)16.1 (R)5.6 ( +)9.8 ( n)14.8 (i)-1.8 (t)10.1 (r)-0.4 (a)14.8 (t)-0.9 (e)]TJ /TT0 1 Tf 0 Tc 0 Tw 12 0 0 12 194.94 256.1401 Tm ( )Tj /TT1 1 Tf -0.0005 Tc 4.9763 0 0 4.9763 351.96 290.8201 Tm [(-)-5.1 (1)13.1 (.8)-2217.5 (-)7 (1)1 (.6)-2217.5 (-)-5.1 (1)13.1 (.4)-2217.5 (-)7 (1)1 (.2)-2205.4 (-)-5.1 (1)1 (.)12.1 (0)-2217.5 (-)-5.1 (0)13.1 (.8)-2217.5 (-)-5.1 (0)1 (.)12.1 (6)-2217.5 (-)7 (0)1 (.4)]TJ -0.00751 Tc -3.9065 1.049 Td [(-0)-6 (.)-7 (1)6.1 (6)]TJ 0 2.8214 TD [(-0)-6 (.)-7 (1)6.1 (4)]TJ 0 2.8093 TD [(-0)-6 (.)-7 (1)6.1 (2)]TJ T* [(-0)-6 (.)-7 (1)6.1 (0)]TJ 0 2.8214 TD [(-0)-6 (.)-7 (0)6.1 (8)]TJ 0 2.8093 TD [(-0)-6 (.)-7 (0)6.1 (6)]TJ T* [(-0)-6 (.)-7 (0)6.1 (4)]TJ T* [(-0)-6 (.)-7 (0)6.1 (2)]TJ -0.00101 Tc 0.3256 2.8214 Td [(0.0)12.6 (0)]TJ T* [(0.0)12.6 (2)]TJ ET 1 0 0 1 346.44 297.3 cm 0 G 0.468 w 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.72 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 9.78 0 cm 0 0 m 0 2.52 l S 1 0 0 1 9.78 0 cm 0 0 m 0 1.26 l S 1 0 0 1 -156.42 0 cm 0 0 m 156.42 0 l S 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.52 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 6.96 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 7.02 cm 0 0 m 2.52 0 l S 1 0 0 1 0 7.02 cm 0 0 m 1.26 0 l S 1 0 0 1 0 6.96 cm 0 0 m 2.52 0 l S 1 0 0 1 0 -126 cm 0 0 m 0 126 l 0 126 l S 1 0 0 1 9.78 126 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.72 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 9.78 0 cm 0 0 m 0 0 l S 1 0 0 1 -156.42 0 cm 0 0 m 156.42 0 l S 1 0 0 1 156.42 -126 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 7.02 cm 0 0 m 0 0 l S 1 0 0 1 0 6.96 cm 0 0 m 0 0 l S 1 0 0 1 0 -126 cm 0 0 m 0 126 l S 1 0 0 1 -9.78 111.9 cm 0.32401 w 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.12 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.12 cm 0 0 m -1.44 0 l S 1 0 0 1 -4.74 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.12 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.18 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.18 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.74 -0.24 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.8 -0.36 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.74 -0.6 cm 0 0 m -1.44 -0.24 l S 1 0 0 1 -4.8 -0.96 cm 0 0 m -1.44 -0.42 l S 1 0 0 1 -4.8 -1.68 cm 0 0 m -1.44 -0.72 l S 1 0 0 1 -4.74 -2.58 cm 0 0 m -1.44 -0.96 l S 1 0 0 1 -4.74 -3.36 cm 0 0 m -1.44 -1.14 l S 1 0 0 1 -4.8 -4.02 cm 0 0 m -1.44 -1.26 l S 1 0 0 1 -4.74 -4.44 cm 0 0 m -1.44 -1.44 l S 1 0 0 1 -4.8 -4.92 cm 0 0 m -1.32 -1.44 l S 1 0 0 1 -4.8 -5.34 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 -4.74 -5.64 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 -4.8 -5.82 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 -4.74 -5.82 cm 0 0 m -1.2 -1.44 l S 1 0 0 1 114.54 46.86 cm 0 0 m -2.4 0 l -7.2 -0.12 l -11.94 -0.12 l -14.34 -0.18 l -16.68 -0.18 l -23.88 -0.36 l -26.28 -0.48 l -28.62 -0.66 l -31.02 -0.72 l -38.22 -1.08 l -40.56 -1.14 l -45.36 -1.38 l -47.76 -1.62 l -50.1 -1.92 l -52.5 -2.46 l -54.9 -3.36 l -57.3 -4.98 l -59.7 -7.8 l -62.04 -12.06 l -64.44 -17.7 l -66.84 -24.3 l -69.24 -31.56 l -71.64 -39.24 l -73.98 -46.8 l -76.38 -53.58 l -78.78 -59.22 l -81.12 -63.3 l -83.52 -65.7 l -85.92 -66.72 l -88.32 -66.54 l -90.66 -65.64 l -93.06 -64.26 l -95.46 -62.76 l -97.86 -61.2 l -100.26 -59.94 l -102.6 -58.98 l -105 -58.14 l -107.4 -57.48 l -109.8 -57.24 l -112.2 -57.36 l -114.54 -57.96 l -116.94 -58.86 l -119.34 -60.12 l S 1 0 0 1 0 -0.06 cm 0.5 G 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.06 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.8 -0.12 cm 0 0 m -1.44 -0.06 l S 1 0 0 1 -4.74 -0.24 cm 0 0 m -1.44 -0.12 l S 1 0 0 1 -4.8 -0.42 cm 0 0 m -1.44 -0.18 l S 1 0 0 1 -4.74 -0.66 cm 0 0 m -1.44 -0.24 l S 1 0 0 1 -4.8 -0.66 cm 0 0 m -1.44 -0.18 l S 1 0 0 1 -4.8 -0.6 cm 0 0 m -1.44 -0.24 l S 1 0 0 1 -4.74 -0.84 cm 0 0 m -1.44 -0.36 l S 1 0 0 1 -4.8 -1.44 cm 0 0 m -1.44 -0.6 l S 1 0 0 1 -4.74 -2.22 cm 0 0 m -1.44 -0.9 l S 1 0 0 1 -4.8 -3.12 cm 0 0 m -1.44 -1.2 l S 1 0 0 1 -4.74 -4.08 cm 0 0 m -1.44 -1.44 l S 1 0 0 1 -4.8 -4.92 cm 0 0 m -1.26 -1.44 l S 1 0 0 1 -4.8 -5.46 cm 0 0 m -1.14 -1.44 l S 1 0 0 1 -4.74 -5.88 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -4.74 -6.06 cm 0 0 m -1.14 -1.44 l S 1 0 0 1 -2.34 -3.06 cm 0 0 m -0.06 -0.06 l S 1 0 0 1 -2.46 -3.3 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.34 -3.06 cm 0 0 m 0 -0.06 l S 1 0 0 1 -2.4 -3.3 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.28 -3.06 cm 0 0 m -0.06 -0.18 l S 1 0 0 1 -2.52 -3.42 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.28 -3.12 cm 0 0 m -0.06 -0.12 l S 1 0 0 1 -2.52 -3.42 cm 0 0 m -1.02 -1.44 l S 1 0 0 1 -2.22 -3.06 cm 0 0 m -0.12 -0.18 l S 1 0 0 1 -2.52 -3.54 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.28 -3.06 cm 0 0 m -0.12 -0.12 l S 1 0 0 1 -2.52 -3.42 cm 0 0 m -1.02 -1.44 l S 1 0 0 1 -2.22 -3.06 cm 0 0 m -0.12 -0.18 l S 1 0 0 1 -2.52 -3.42 cm 0 0 m -1.08 -1.44 l S 1 0 0 1 -2.34 -3.12 cm 0 0 m 0 -0.06 l S 1 0 0 1 116.88 85.2 cm 0 0 m -2.4 0 l -4.8 -0.06 l -7.2 -0.06 l -9.54 -0.12 l -11.94 -0.18 l -14.34 -0.18 l -16.68 -0.3 l -21.48 -0.42 l -23.88 -0.54 l -26.28 -0.78 l -28.62 -0.9 l -31.02 -1.14 l -35.82 -1.86 l -38.22 -2.16 l -40.56 -2.4 l -45.36 -3.24 l -47.76 -3.78 l -50.1 -4.56 l -52.5 -5.58 l -54.9 -7.08 l -57.3 -9.42 l -59.7 -12.84 l -62.04 -17.76 l -64.44 -24.06 l -66.84 -31.56 l -69.24 -39.84 l -71.64 -48.3 l -73.98 -56.64 l -76.38 -64.08 l -78.78 -70.08 l -81.12 -74.1 l -83.52 -76.14 l -85.92 -76.5 l -88.32 -75.48 l -90.66 -73.56 l -93.06 -70.92 l -95.46 -68.58 l -97.86 -67.2 l -100.26 -66.9 l -102.6 -67.14 l -105 -67.62 l -107.4 -68.22 l -109.8 -68.94 l -112.2 -70.26 l -114.54 -72.6 l -116.94 -75.72 l -119.34 -79.44 l S 1 0 0 1 -493.08 -409.14 cm BT /TT2 1 Tf -0.0088 Tc 6.1071 0 0 6.1071 362.58 407.7 Tm [(\(b)12.6 (\))]TJ /TT1 1 Tf 0 Tc 10.031 3.6351 Td ( )Tj 0 6.1071 -6.1071 0 513.78 355.44 Tm ( )Tj 0.0016 Tc -0.0043 Tw -2.7214 30.4072 Td [(Cu)-12.1 (rrent)-5.5 ( / )-9.8 (mA)]TJ 0.00369 Tc -0.00639 Tw 6.1071 0 0 6.1071 376.2 280.92 Tm [(Pot)6.4 (ent)6.4 (ial / V )]TJ /TT3 1 Tf 0.0024 Tc 0 Tw 5.6885 0 Td [(vers)-8.5 (us)]TJ /TT1 1 Tf 0.0015 Tc -0.0042 Tw 2.967 0 Td ( Ag/AgCl/KCl)Tj 0 Tw 3.6513 0 0 3.6513 464.82 278.5201 Tm [(\()5.9 (s)-7.9 (a)15.4 (t.\))]TJ ET 1 0 0 1 408.3 327.24 cm 0 G 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 -420.54 -327.24 cm BT /TT1 1 Tf -0.00529 Tc 0.0098 Tw 5.5254 0 0 5.5254 422.34 325.38 Tm [( BDUND_B)-11.6 (u)-3 (f)-9.8 (f)-9.8 (e)-3 (r BR)]TJ ET 1 0 0 1 408.3 320.52 cm 0 0 m 14.04 0 l S 1 0 0 1 -408.3 -320.52 cm BT /TT1 1 Tf -0.0047 Tc 0.0092 Tw 5.5254 0 0 5.5254 422.34 318.6 Tm [( BDUND_B)-11 (u)-2.4 (f)-9.2 (f)-9.2 (e)-2.4 (r BR +)-7.1 ( nit)-9.2 (r)-8.3 (at)-9.2 (e)]TJ ET 1 0 0 1 408.3 313.74 cm 0.5 G 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 3.06 0 cm 0 0 m 1.44 0 l S 1 0 0 1 -420.54 -313.74 cm BT /TT1 1 Tf -0.0051 Tc 0.0096 Tw 5.5254 0 0 5.5254 422.34 311.88 Tm [( Cu/)-9.6 (B)-0.5 (DUND_B)-11.4 (u)-2.8 (f)-9.6 (f)-9.6 (e)-2.8 (r BR)]TJ ET 1 0 0 1 408.3 307.02 cm 0 0 m 14.04 0 l S 1 0 0 1 -408.3 -307.02 cm BT /TT1 1 Tf -0.00459 Tc 0.00909 Tw 5.5254 0 0 5.5254 422.34 305.1 Tm [( Cu/)-9.1 (BDUND_B)-10.9 (u)-2.3 (f)-9.1 (f)-9.1 (e)-2.3 (r BR +)-7 ( nit)-9.1 (r)-8.2 (at)-9.1 (e)]TJ /TT0 1 Tf 0 Tc 0 Tw 12 0 0 12 416.34 254.7001 Tm ( )Tj /TT4 1 Tf 0.0004 Tc 0.03461 Tw -27.195 -1.15 Td (Figure 3.)Tj /TT0 1 Tf 0.0097 Tw 3.87 0 Td [( T)6.1 (h)0.3 (e response of diam)8.1 (ond electrodes for 0.001 m)8.1 (o)0.3 (l L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 392.58 246.4201 Tm (-1)Tj -0.0005 Tc 0.0105 Tw 12 0 0 12 399.24 240.9001 Tm ( BR buffer and for nitrate )Tj 0.00031 Tc 0.04469 Tw -25.77 -1.15 Td [(reduction in solution of 0.01 m)8.1 (o)0.3 (l L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 261.54 232.6201 Tm (-1)Tj 0.0472 Tw 12 0 0 12 268.26 227.1001 Tm ( KNO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 297.72 225.6001 Tm (3)Tj 0.0011 Tc 0.0451 Tw 12 0 0 12 301.74 227.1001 Tm [( + 0.001 m)8.9 (o)1.1 (l L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 375.72 232.6201 Tm (-1)Tj 0.00011 Tc 0.0457 Tw 12 0 0 12 382.38 227.1001 Tm ( BR buffer. \(a\) BDD and \(b\) )Tj -0.0013 Tc 0 Tw -24.365 -1.15 Td [(BDUND.)-6.3 ( )]TJ 0 Tc 1.49 -1.15 Td ( )Tj 0 -1.15 TD ( )Tj 0.0183 Tw T* (In Figure 3 \(a\), it is possible )Tj -0.0007 Tc 0.02071 Tw 11.68 0 Td [(to observe the appearance of )-1.8 (a slight new peak at around )]TJ 0.0002 Tc 0.0948 Tw -13.17 -1.15 Td [(-1.0 V associated to the nitrate reducti)-1.2 (on into hydroxylam)8 (ine followed by the ammonia )]TJ -0.0002 Tc 0.37891 Tw T* (peak. These reduction processes we)Tj -0.00031 Tc 0.38029 Tw 15.815 0 Td (re already observed by Aouina )Tj /TT5 1 Tf 0.00169 Tc 0.3783 Tw 14.42 0.005 Td [(et a)6.7 (l)]TJ /TT0 1 Tf -0.00281 Tc 0.3828 Tw 2.13 -0.005 Td [( for t)-5 (h)2.2 (e )]TJ 0.0002 Tc 0.0798 Tw -32.365 -1.15 Td (electroreduction of nitrate at )Tj 0.0004 Tc 0.07829 Tw 11.925 0 Td (a copper electrode in neutral )Tj 0.0005 Tc 0.0757 Tw 12.035 0 Td (solution \(16\). In addition, the )Tj 0.00079 Tc 0.2442 Tw -23.96 -1.15 Td [(stability of)3.8 ( Cu partic)4.6 (les)5 ( on these f)3.8 (ilm)8.6 (s )]TJ 0.0006 Tc 0.2444 Tw 17.185 0 Td [(was evaluated from successiv)5.6 (e)-0.6 ( linear sweep )]TJ 0.1194 Tw -17.185 -1.15 Td [(voltamm)8.4 (etry m)8.4 (easurem)8.4 (e)-5.6 (n)0.6 (ts for the nitrate re)]TJ 0.0005 Tc 0.1188 Tw 18.405 0 Td [(duction, show)7.7 (n in Figure 4 \(a\) and \(b\) for )]TJ 0 Tc -0.00121 Tw -18.405 -1.15 Td (Cu/BDD and Cu/BDUND, respectively. )Tj ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_1 10 Tf 0 Tw 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_1 10 Tf 0 Tw 298.5 12 Td (181)Tj ET Q BT /GS1 gs /T1_2 1 Tf 0 Tw 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_3 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_2 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_3 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_2 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 25 0 obj <> endobj 22 0 obj <> endobj 24 0 obj <> endobj 23 0 obj <>stream hTP=O0+n,bGRT2)} m9ΐm"}wG9E{L0Xg"~ኣuU'fr S\awk4aw9/!|.)@h{VEMb5 m781*7"4LHhϑ/:/Vɟx1? ~eJ c#֥L)%ƼKO\Zȏ3q endstream endobj 2 0 obj <>stream HNJPJN+Symbol' H \cjs v|asteriskmathnupiarrowrightCopyright (c) 1985, 1987, 1989, 1990, 1997 Adobe Systems Incorporated. All rights reserved.Symbol *np1 طrgd}{qkkkfͪwkrxuznQm|ŐUUNcQu|Qurk|wirlfkkkqk{{ɯwIraow5vmwQrExg?J4rxdua~\KsnS<,Q{%z5W;dgqxv|orxkrn~|ۗ  ]loszmab}nyant{v{x{ituOv"pde7%[Oh-E4hhO%ex5]  endstream endobj 91 0 obj <> endobj 104 0 obj <> endobj 105 0 obj <> endobj 106 0 obj <> endobj 86 0 obj [107 0 R 108 0 R] endobj 87 0 obj <>stream q 84.6 737.88 219.48 -176.28 re W* n q 0 792.03 612 -792 re W n q /GS0 gs 175.5 0 0 175.5 106.56 562.38 cm /Im0 Do Q Q Q q 304.08 737.88 219.54 -176.28 re W* n q 0 792.03 612 -792 re W n q /GS0 gs 176.28 0 0 176.28 325.68 561.6 cm /Im1 Do Q Q Q BT /GS0 gs /TT0 1 Tf 0.0004 Tc 0.32961 Tw 12 0 0 12 90 550.5601 Tm (Figure 2.)Tj /TT1 1 Tf 0.3054 Tw 4.165 0 Td [( SEM i)-6.9 (m)8.1 (ages of B)-2.7 (D)2.5 (D \(a\) and BDUND )]TJ 0.00079 Tc 0.3042 Tw 18.39 0 Td [(\(b\) electrodes af)8.8 (ter Cu particle )]TJ 0.0004 Tc -0.0054 Tw -22.555 -1.15 Td (photoelectrodeposits. )Tj 0 Tc 0 Tw 1.49 -1.15 Td ( )Tj 0 -1.15 TD ( )Tj 0.3085 Tw T* [(According to Figure 2 \(a\), the B)7 (DD exhi)]TJ 0.00011 Tc 0.30901 Tw 18.435 0 Td (bits the highest density and the best )Tj 0.0004 Tc 0.1846 Tw -19.925 -1.15 Td [(uniform)8.2 (ness of Cu particles on the electr)]TJ 0.0002 Tc 0.1833 Tw 17.39 0 Td [(ode s)4.4 (u)0.2 (rface. For the BDUND \(im)8 (a)-1 (ge b\) the )]TJ 0.0006 Tc 0.0544 Tw -17.39 -1.15 Td [(electrodeposits seem)8.4 ( larger and at the clus)]TJ 0 Tc 0.05499 Tw 17.225 0 Td [(ter grain boundaries of the BDUND. The)-6.1 (y are )]TJ 0.0002 Tc 0.44479 Tw -17.225 -1.15 Td [(random)8 (ly located, with low particle density. The strong difference between the\ )]TJ 0.00031 Tc -0.00031 Tw T* [(electrodeposits in both electrodes m)8.1 (a)-5.9 (y be expl)2 (ained due to the sem)8.1 (i)-1.9 (conductor character of )]TJ 0.0002 Tc 0.0139 Tw T* [(such film)8 (s. Firstly, the BDD surfac)-6 (e presen)]TJ 0 Tc 0.01579 Tw 17.415 0 Td [(ts high diam)7.8 (ond purity where the conductivity )]TJ 0.0004 Tc 0.0291 Tw -17.415 -1.15 Td (is due to the boron excess at the top of its )Tj 0.0002 Tc 0.0298 Tw 17.145 0 Td (valence band. So, the photoassisted process by )Tj -0.00031 Tc 0.0453 Tw -17.145 -1.15 Td [(UV irradiation generates additi)-9.6 (onal electrons at the conducti)]TJ -0.00011 Tc 0.0451 Tw 24.44 0 Td [(on band that m)7.7 (a)-1.3 (y participate )]TJ 0.0006 Tc 0.0094 Tw -24.44 -1.15 Td [(in the)4.4 ( Cu ele)4.4 (c)-0.6 (tror)3.6 (eductio)5.6 (n. In add)5.6 (itio)5.6 (n, the pos)4.8 (itive holes)4.8 ( at the valen)5.6 (ce b)5.6 (a)-0.6 (nd m)8.4 (a)-0.6 (y oxidize)4.4 ( )]TJ 0.0869 Tw T* [(the water to m)8.4 (o)0.6 (lecular oxygen )]TJ 0.00011 Tc 0.0882 Tw 12.855 0 Td (or hydroxyl radicals. Also, )Tj -0.00031 Tc 0.089 Tw 11.295 0 Td (BDD represents a wide band )Tj 0.0004 Tc 0.0536 Tw -24.15 -1.15 Td [(gap sem)8.2 (i)-1.8 (conductor. This process is improve)]TJ 0.0546 Tw 17.885 0 Td [(d due to the large BDD band gap, where the)-5.7 ( )]TJ 0.03461 Tw -17.885 -1.15 Td [(recom)8.2 (b)0.4 (ination of the electrons )]TJ 0.0006 Tc 0.0329 Tw 12.575 0 Td [(is lower com)8.4 (p)0.6 (ared to that of)8.6 ( conventional sem)8.4 (i)-1.6 (conductors )]TJ 0.2074 Tw -12.575 -1.15 Td (\(14\). In this way, this ex)Tj 0.00031 Tc 0.20799 Tw 10.8 0 Td (cess of electrons enhanced )Tj 0 Tc 0.20869 Tw [0.2 (the Cu deposition. The possible )]TJ 0.0002 Tc -0.00101 Tw -10.8 -1.15 Td [(reactions that m)8 (a)-1 (y occurs in this photoassi)]TJ 0.0005 Tc -0.0013 Tw 16.945 0 Td [(s)4.7 (t)-1.7 (ed process is summ)8.3 (arized in Table 1.)5.5 ( )]TJ 0 Tc 0 Tw -15.455 -1.15 Td ( )Tj T* ( )Tj /TT0 1 Tf 0.0002 Tc 0.11481 Tw -1.49 -1.15 Td (Table 1-)Tj /TT1 1 Tf 0.0004 Tc 0.08859 Tw 3.645 0 Td ( Possible reactions in the photocataly)Tj 0.00011 Tc 0.0899 Tw 15.315 0 Td [(tic process of the diam)7.9 (ond in 1 mmol L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 515.4 280.08 Tm (-1)Tj 0 Tc 12 0 0 12 521.9999 274.5601 Tm ( )Tj -0.0011 Tc -36 -1.15 Td (CuSO)Tj 0 Tc 7.98 0 0 7.98 119.28 259.2601 Tm (4)Tj 0.00011 Tc -0.00011 Tw 12 0 0 12 123.3 260.7601 Tm ( + 50 mmol L)Tj -0.0022 Tc 0 Tw 7.98 0 0 7.98 189.36 266.2801 Tm (-1)Tj 0 Tc 12 0 0 12 196.02 260.7601 Tm ( H)Tj 7.98 0 0 7.98 207.66 259.2601 Tm (2)Tj -0.00121 Tc 12 0 0 12 211.74 260.7601 Tm (SO)Tj 0 Tc 7.98 0 0 7.98 227.04 259.2601 Tm (4)Tj 12 0 0 12 231.06 260.7601 Tm ( aqueous solution. )Tj -0.0011 Tc -11.755 -1.77 Td (CuSO)Tj 0 Tc 7.98 0 0 7.98 119.28 238.0201 Tm (4)Tj 12 0 0 12 123.3 239.5201 Tm ( )Tj /T1_0 1 Tf (\002)Tj /TT1 1 Tf -0.0013 Tc 0.0038 Tw 1.485 0 Td ( Cu)Tj 0.0038 Tc 0 Tw 7.98 0 0 7.98 161.16 245.0401 Tm (2+)Tj -0.00011 Tc 0.00011 Tw 12 0 0 12 169.68 239.5201 Tm ( + SO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 203.76 238.0201 Tm (4)Tj 0.0038 Tc 0.5038 0.8797 Td (2-)Tj 0 Tc 12 0 0 12 214.44 239.5201 Tm ( )Tj -0.00101 Tc 20.83 0.08 Td (\(1\) )Tj ET 84.6 257.52 432.18 0.48001 re f BT /TT1 1 Tf 0 Tc 12 0 0 12 90 212.8201 Tm (H)Tj 7.98 0 0 7.98 98.64 211.3201 Tm (2)Tj -0.00121 Tc 12 0 0 12 102.66 212.8201 Tm (SO)Tj 0 Tc 7.98 0 0 7.98 117.96 211.3201 Tm (4)Tj 12 0 0 12 121.98 212.8201 Tm ( )Tj /T1_0 1 Tf (\002)Tj /TT1 1 Tf 0.0013 Tc 0.00121 Tw 1.485 0 Td ( 2H)Tj 0 Tc 0 Tw 7.98 0 0 7.98 160.5 218.3401 Tm (+)Tj -0.00011 Tc 0.00011 Tw 12 0 0 12 165 212.8201 Tm ( + SO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 199.08 211.3201 Tm (4)Tj 0.0038 Tc 0.5038 0.8797 Td (2-)Tj 0 Tc 12 0 0 12 209.76 212.8201 Tm ( )Tj -0.00101 Tc 21.22 0.08 Td (\(2\) )Tj 0 Tc -31.2 -2.305 Td (H)Tj 7.98 0 0 7.98 98.64 184.6201 Tm (2)Tj -0.0022 Tc 0.0022 Tw 12 0 0 12 102.66 186.1201 Tm (O )Tj /T1_0 1 Tf 0 Tc 0 Tw [-0.2 (\002)]TJ /TT1 1 Tf 2.205 0 Td ( H)Tj 7.98 0 0 7.98 143.76 191.64 Tm (+)Tj 0.0004 Tc 0.00079 Tw 12 0 0 12 148.26 186.1201 Tm ( + OH)Tj 0 Tc 0 Tw 7.98 0 0 7.98 184.38 191.64 Tm (-)Tj 12 0 0 12 187.08 186.1201 Tm ( )Tj -0.00101 Tc 23.11 0.08 Td (\(3\) )Tj 0 Tc -31.2 -2.305 Td (h)Tj /T1_0 1 Tf (\003)Tj /TT1 1 Tf 1.02 0 Td ( )Tj /T1_0 1 Tf (\002)Tj /TT1 1 Tf 1.485 0 Td ( h)Tj 7.98 0 0 7.98 132.06 164.94 Tm (+)Tj 12 0 0 12 136.56 159.42 Tm [( +)-6 ( e)]TJ 7.98 0 0 7.98 160.74 164.94 Tm (-)Tj 12 0 0 12 163.38 159.42 Tm ( )Tj -0.00101 Tc 25.085 0.08 Td (\(4\) )Tj -0.002 Tc -31.2 -2.305 Td (Cu)Tj 0.0038 Tc 7.98 0 0 7.98 103.98 138.2401 Tm (2+)Tj 0.00031 Tc -0.00031 Tw 12 0 0 12 112.5 132.7201 Tm ( + 2e)Tj 0 Tc 0 Tw 7.98 0 0 7.98 142.62 138.2401 Tm (-)Tj 12 0 0 12 145.26 132.7201 Tm ( )Tj /T1_0 1 Tf (\002)Tj /TT1 1 Tf 0.00079 Tc -0.00079 Tw 1.485 0 Td ( Cu )Tj -0.00101 Tc 0 Tw 25.11 0.08 Td (\(5\) )Tj 0 Tc -31.2 -2.305 Td (2 H)Tj 7.98 0 0 7.98 107.64 111.54 Tm (+)Tj 0.00031 Tc -0.00031 Tw 12 0 0 12 112.14 106.0201 Tm ( + 2e)Tj 0 Tc 0 Tw 7.98 0 0 7.98 142.26 111.54 Tm (-)Tj 12 0 0 12 144.9 106.0201 Tm ( )Tj /T1_0 1 Tf 0.505 0 Td (\002)Tj /TT1 1 Tf 0.985 0 Td ( H)Tj 7.98 0 0 7.98 177.42 104.5201 Tm (2)Tj 12 0 0 12 181.44 106.0201 Tm ( )Tj -0.00101 Tc 23.58 0.08 Td (\(6\) )Tj -0.0022 Tc -31.2 -2.305 Td (OH)Tj 0 Tc 7.98 0 0 7.98 107.28 84.8401 Tm (-)Tj 0.0004 Tc -0.0004 Tw 12 0 0 12 109.92 79.32 Tm ( + h)Tj 0 Tc 0 Tw 7.98 0 0 7.98 134.7 84.8401 Tm (+)Tj 12 0 0 12 139.2 79.32 Tm ( )Tj /T1_0 1 Tf 0.505 0 Td (\002)Tj /TT1 1 Tf 0.985 0 Td ( )Tj /TT2 1 Tf (\225)Tj /TT1 1 Tf 0.00031 Tc (OH )Tj -0.00101 Tc 25.61 0.08 Td (\(7\) )Tj ET 83.88 70.08 375.12 0.48001 re f 458.28 70.08 58.5 0.48001 re f BT /TT1 1 Tf 0 Tc 12 0 0 12 107.88 59.04 Tm ( )Tj ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_1 10 Tf 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_1 10 Tf 298.5 12 Td (180)Tj ET Q BT /GS1 gs /T1_2 1 Tf 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_3 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_2 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_3 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_2 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 30 0 obj <>stream hޔ{ #m$EivO3vMbT@}ދޝ꣛BUa+m۾?jǎ?]Mg!^4?*oc>Zuzk͞(x}ڎ>Knz}vcg?îy#asN_1kkkqauq.nm ,T%QobŹ' 7k۴g>KWGaԪk۴(;QuۯofeKd+hϜSaA6fU/.~€@|.;B}6Zֿd<EsSov "8>:xǯ?E4:5_M;8$%3eX`_|M>gkM#߸K.Zyk`3\|0>fZ )!b d+{-^ \}wSo[9SO>r|qe!?M;T?,?4[v~/!`˝,qc6nS\# ZVID-i/}C2 g w6`CUi~·}^Ma3=Zm;*(+"EW@ zY9(PjS5f (cp|ꁿe5~)^[t0Î\abTHX o16U熖OgM+^s/ [!o+v4nn+vY?U`yϏ~cZ}%BΏ^fW?Jgh&%OG`yBb!&F {0Gbkcy'u[Zj m8Kja@%*vn_aYFWVkz -Eɼl(Ćx>w(gG;6,%W.hU^%k :qz[\5,#l=s  @~tOހ]*e+嶨a652J0nTeQɨtĸV 1GP6ǡ*h8pɂ%[P#y/^Qdؗ}/kPٿIYK P+ni?#h]I$޲x绲$=Ԣ+~U0&bBs3 Q@} *L*dFSwJG0gݖ~]"&c"uYoJцZ~#߳uhKXkzKDaPG*dq x?&.=qMOe 2jFh{${a^=,\! >,KoUj 5bY4hnOM透Ba`w7L۷|hJ,kLqv~)2ܽ*` 3TjY w;-2E&ė,hkr=V`3RJp+v}*ՍXFfr-Je=,Ƒxu{ _bA+¤ Zִ rs#hEۘȊ}0Ody!!=0op0N#{'Zq"(5 :;"Eo MFX*IeΞF7BsM\GR$" ¶xyhV-bKe9tX(ꞋtH aK1H:|9*T 蓡](5O EES6CAmE$ZcU H!8I8٧o ny;fLk~l&HK8⋳Ӭ H)RE*F n ,<zF<2pIJJEjv8n%CJ˜|䎞 "U蛱ҝ ~OD.-@%(žݛ^ȯfծd6#yo:!>|d=P``i=S[GKɍKN)u--v&ZBfǕc 5`'CwݖK}iWAg9{&E[ybw]ubVBWi-5ZvѽpfDfhYK&~r5ʇpaLy$W)ZoOnM(8x!:axDB" W M*ڴR_-b2svllD,R9HA# TOaޝ?y,+$/xi%$,:h{hkU^,*~\HXn'8@a̯D&8W/B݊sTnvPG C\Dp}i⧬K#_36tUB; Am=-$JLHmJIyK+>;4tJWboAj.p:\1$wtG|^zspE"ފlL9hOzS*OB#]!_"D|z4r.B x5s@Dz}zD?yHzh V)4+Z$ђ2bw!V-~y;N p&& ˫_a#Ҟhx i0ŕR5}բJOV!/roCwͷ;`c!$\h``'5a^ }py4Mn/ [҄Ul1 U oXΘ [a+Di nNŐnVKbd>lby#l=@:S7T~Ƣ{)Z[]< x=cxke"h[10tU[?+,# #7E/Kl]^̫۠D$:d+l6=ޠ7 vN[0 d8I3 +nHje9lKe_ѵ1XȿZ5cn]3@Ιp^Ue ]1CKsg+Dو< ĿEXMi--xA3@)!,ҋTJ3M×!3  $cs hev_A];~CHCy>'3p#te!V`jf┑ë0|guKD; lP= LOWLX$S*p/ eH$7K|]ʎx?Ԩ In)YZRm坓 _o=K򌪞&Л+wGk8lsdKltOڗ|l}~{*ƪ*5~9 9AıR2Ga10naYҍBjnO5tjy\78vhfkA% Z1o+u5wV[ƒ^Ӆq!`So]l;/:#E#q@NFv#!܄T1ԒEltU*_,Ԅ^V*i69яFLuOgt-+uBfD@캮(K M"G$!g90SjY"9fٿM$?Rm汼8z^|shl V 2I~{ @rſ , #nI3czF?X/%sjʩI}z%0`vk W\gb*#;n@ u+9V416*G Ko;z[N`_νthdwgExq_[ ?s3:}|}bf wQ͙MzlUÔY8:CsunZdwaTAy!,sIxxI k[)У2 8g{"TYJ}R-1qO9/R3WaNHXY֮0 IԹPSUC˘Wb'5$\U=_/+!7_ Paiސe:Fؿ=_ z_h"vb:zҺA/IN{ z>|s.j}d@_yVՏ ꫦǻ+=D֓LT7{ssʠOT4LjVGN&@'nGȹ<@ KE 91!=LY9~%LfzKarl* cr^:!`Eid6.=K nO3>S.JF^Sda1)quvĀ^'}!!bC`Oʼn;$gcCdclɳuCO1x~N?3!c)\[b ؑՒOf5M\Zj >F'1a:= (1#E8w8<[4l_٧€y ɛX(l>W(pvK '2/F;59񽡷_Zz(׋=oZ 豽ihE?M`K5"AsԪzcEGʘr^if 9?u+4O\p1 ׿{_-2߿? 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0 0 1 -2.04 1.14 cm 0 0 m -0.84 0.42 l S 1 0 0 1 -1.98 0.84 cm 0 0 m -0.9 0.36 l S 1 0 0 1 -1.98 0.6 cm 0 0 m -0.9 0.24 l S 1 0 0 1 -1.98 0.54 cm 0 0 m -0.9 0.06 l S 1 0 0 1 -2.04 0.3 cm 0 0 m -0.84 0.12 l S 1 0 0 1 -1.98 0.3 cm 0 0 m -0.9 0.18 l S 1 0 0 1 -1.98 0.24 cm 0 0 m -0.9 0.18 l S 1 0 0 1 -2.04 0.24 cm 0 0 m -0.84 0.12 l S 1 0 0 1 -1.98 0.3 cm 0 0 m -0.84 0.12 l S 1 0 0 1 -1.98 0.24 cm 0 0 m -0.9 0.06 l S 1 0 0 1 -1.98 0.24 cm 0 0 m -0.9 0.12 l S 1 0 0 1 -2.04 0.18 cm 0 0 m -0.84 0.18 l S 1 0 0 1 -1.98 0.18 cm 0 0 m -0.96 0.06 l S 1 0 0 1 -1.98 0.06 cm 0 0 m -0.96 0 l S 1 0 0 1 -1.98 -0.06 cm 0 0 m -0.9 -0.12 l S 1 0 0 1 -2.04 -0.42 cm 0 0 m -0.84 -0.42 l S 1 0 0 1 -1.98 -1.14 cm 0 0 m -0.96 -0.84 l S 1 0 0 1 -1.98 -2.22 cm 0 0 m -0.6 -1.02 l S 1 0 0 1 -2.04 -3.96 cm 0 0 m -0.36 -1.02 l S 1 0 0 1 -0.78 -2.22 cm 0 0 m -0.18 -0.54 l S 1 0 0 1 -1.2 -4.08 cm 0 0 m -0.24 -1.02 l S 1 0 0 1 -0.54 -2.22 cm 0 0 m -0.24 -1.02 l S 1 0 0 1 -1.44 -6.18 cm 0 0 m -0.18 -1.08 l S 1 0 0 1 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l S 1 0 0 1 2.04 2.22 cm 0 0 m 0.9 0.78 l S 1 0 0 1 1.98 1.56 cm 0 0 m 0.9 0.48 l S 1 0 0 1 1.98 1.08 cm 0 0 m 0.96 0.48 l S 1 0 0 1 1.98 0.72 cm 0 0 m 0.96 0.42 l S 1 0 0 1 2.04 0.66 cm 0 0 m 0.9 0.18 l S 1 0 0 1 1.98 0.36 cm 0 0 m 0.96 0.18 l S 1 0 0 1 1.98 0.24 cm 0 0 m 0.96 0.12 l S 1 0 0 1 1.98 0.18 cm 0 0 m 0.96 0.18 l S 1 0 0 1 2.04 0.18 cm 0 0 m 0.9 0.12 l S 1 0 0 1 1.98 0.18 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 0.06 cm 0 0 m 0.96 0.12 l S 1 0 0 1 2.04 0.12 cm 0 0 m 0.9 0.06 l S 1 0 0 1 1.98 0.18 cm 0 0 m 0.9 0 l S 1 0 0 1 1.98 0.06 cm 0 0 m 0.96 0.12 l S 1 0 0 1 1.98 0.12 cm 0 0 m 0.96 0.06 l S 1 0 0 1 2.04 0.06 cm 0 0 m 0.9 0.06 l S 1 0 0 1 1.98 0.18 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 0.06 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 0.12 cm 0 0 m 0.96 0 l S 1 0 0 1 2.1 0.06 cm 0 0 m 0.84 0 l S 1 0 0 1 1.92 0 cm 0 0 m 0.96 0.12 l S 1 0 0 1 1.98 0.12 cm 0 0 m 0.96 0 l S 1 0 0 1 2.1 0 cm 0 0 m 0.84 0.06 l S 1 0 0 1 1.98 0.06 cm 0 0 m 0.84 0 l S 1 0 0 1 1.92 0.12 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 0.06 cm 0 0 m 0.96 0 l S 1 0 0 1 2.1 0.06 cm 0 0 m 0.84 0.12 l S 1 0 0 1 1.98 0.18 cm 0 0 m 0.9 0.12 l S 1 0 0 1 1.92 0.18 cm 0 0 m 0.96 0.12 l S 1 0 0 1 1.98 0.24 cm 0 0 m 0.96 0.18 l S 1 0 0 1 2.1 0.36 cm 0 0 m 0.84 0.18 l S 1 0 0 1 1.98 0.42 cm 0 0 m 0.9 0.36 l S 1 0 0 1 1.92 0.72 cm 0 0 m 0.96 0.36 l S 1 0 0 1 2.1 0.84 cm 0 0 m 0.84 0.54 l S 1 0 0 1 1.98 1.2 cm 0 0 m 0.84 0.9 l S 1 0 0 1 1.98 1.98 cm 0 0 m 0.66 1.02 l S 1 0 0 1 1.92 3.36 cm 0 0 m 0.48 1.02 l S 1 0 0 1 1.08 2.22 cm 0 0 m 0 0 l S 1 0 0 1 1.02 2.76 cm 0 0 m 0.36 1.08 l S 1 0 0 1 0.66 2.28 cm 0 0 m 0.3 0.84 l S 1 0 0 1 1.32 4.44 cm 0 0 m 0.24 1.02 l S 1 0 0 1 0.6 2.22 cm 0 0 m 0.3 1.08 l S 1 0 0 1 1.38 5.52 cm 0 0 m 0.24 1.02 l S 1 0 0 1 0.48 2.28 cm 0 0 m 0.24 1.02 l S 1 0 0 1 1.56 6.36 cm 0 0 m 0.24 1.02 l S 1 0 0 1 0.48 2.22 cm 0 0 m 0.3 1.02 l S 1 0 0 1 1.5 5.1 cm 0 0 m 0.42 1.02 l S 1 0 0 1 0.84 2.22 cm 0 0 m 0.12 0.18 l S 1 0 0 1 1.14 1.62 cm 0 0 m 0.9 -0.42 l S 1 0 0 1 1.98 -4.56 cm 0 0 m 0.06 -1.02 l S 1 0 0 1 0.24 -2.22 cm 0 0 m 0.06 -1.02 l S 1 0 0 1 0.24 -2.22 cm 0 0 m 0.12 -1.08 l S 1 0 0 1 0.24 -2.28 cm 0 0 m 0.12 -1.02 l S 1 0 0 1 0.3 -2.22 cm 0 0 m 0 -0.24 l S 1 0 0 1 1.02 -11.7 cm 0 0 m 0.18 -1.02 l S 1 0 0 1 0.42 -2.22 cm 0 0 m 0.18 -1.08 l S 1 0 0 1 0.36 -2.28 cm 0 0 m 0.18 -0.78 l S 1 0 0 1 1.2 -3.42 cm 0 0 m 0.66 -1.02 l S 1 0 0 1 1.98 -2.52 cm 0 0 m 0.9 -0.48 l S 1 0 0 1 1.98 -1.2 cm 0 0 m 0.9 -0.3 l S 1 0 0 1 2.04 -1.02 cm 0 0 m 0.84 -0.96 l S 1 0 0 1 1.98 -1.98 cm 0 0 m 0.96 -0.6 l S 1 0 0 1 1.98 -1.26 cm 0 0 m 0.9 -0.48 l S 1 0 0 1 2.04 -0.9 cm 0 0 m 0.84 -0.24 l S 1 0 0 1 1.98 -0.48 cm 0 0 m 0.84 -0.18 l S 1 0 0 1 1.98 -0.48 cm 0 0 m 0.96 -0.06 l S 1 0 0 1 1.98 -0.24 cm 0 0 m 0.9 -0.18 l S 1 0 0 1 2.04 -0.24 cm 0 0 m 0.84 -0.18 l S 1 0 0 1 1.98 -0.24 cm 0 0 m 0.96 -0.18 l S 1 0 0 1 1.98 -0.3 cm 0 0 m 0.96 -0.06 l S 1 0 0 1 1.98 -0.18 cm 0 0 m 0.9 -0.06 l S 1 0 0 1 2.04 -0.12 cm 0 0 m 0.84 -0.12 l S 1 0 0 1 1.98 -0.18 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 -0.12 cm 0 0 m 0.96 0 l S 1 0 0 1 2.04 -0.06 cm 0 0 m 0.84 0 l S 1 0 0 1 1.98 -0.12 cm 0 0 m 0.84 0 l S 1 0 0 1 1.98 0 cm 0 0 m 0.96 -0.06 l S 1 0 0 1 1.98 -0.06 cm 0 0 m 0.96 -0.06 l S 1 0 0 1 2.04 -0.06 cm 0 0 m 0.84 0 l S 1 0 0 1 1.98 0 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 -0.12 cm 0 0 m 0.96 0 l S 1 0 0 1 1.98 0 cm 0 0 m 0.96 0 l S 1 0 0 1 2.04 -0.06 cm 0 0 m 0.9 0.06 l S 1 0 0 1 -403.92 -645.72 cm BT /TT0 1 Tf 0 Tc 0 7.2398 -7.2398 0 437.04 629.94 Tm ( )Tj 7.2398 0 0 7.2398 325.56 716.4 Tm ( )Tj -0.0014 Tc -0.0029 Tw 0 7.2398 -7.2398 0 197.82 627 Tm [(C)-8.5 (u)-0.5 (rr)-8.2 (ent / mA)]TJ -0.0032 Tc -0.0011 Tw 7.2398 0 0 7.2398 269.64 543.48 Tm [(Potenti)-13.1 (a)-2.3 (l)-4.8 ( / V )]TJ /TT1 1 Tf -0.0016 Tc 0 Tw 5.6438 0 Td (versus)Tj /TT0 1 Tf -0.00281 Tc -0.0015 Tw 2.9338 0 Td [( Ag)-10.2 (/)9.8 (A)-7.1 (gCl)-4.4 (/)1.5 (KCl)]TJ 0.0004 Tc 0 Tw 4.313 0 0 4.313 373.92 540.66 Tm [(\()27.4 (s)-0.4 (a)14 (t.\))]TJ ET 1 0 0 1 354.18 601.02 cm 0 0 m 16.14 0 l S 1 0 0 1 -354.18 -601.02 cm BT /TT0 1 Tf 0.0043 Tc -0.01691 Tw 7.2398 0 0 7.2398 370.32 598.62 Tm [( BD)5.5 (D)]TJ ET 1 0 0 1 354.18 592.2 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 1.08 0 l S 1 0 0 1 2.28 0 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 1.02 0 l S 1 0 0 1 2.22 0 cm 0 0 m 0.42 0 l S 1 0 0 1 -369.78 -592.2 cm BT /TT0 1 Tf -0.00121 Tc -0.0114 Tw 7.2398 0 0 7.2398 370.32 589.74 Tm [( B)-5.5 (DUND)]TJ /TT2 1 Tf 0 Tc 0 Tw 12 0 0 12 453.96 524.46 Tm ( )Tj /TT3 1 Tf 0.0004 Tc 0.20959 Tw -30.33 -0.925 Td (Figure 1.)Tj /TT2 1 Tf -0.0002 Tc 0.1852 Tw 4.045 0 Td ( Cyclic voltammetry responses BDD a)Tj 0 Tc 0.185 Tw 16.335 0 Td [(nd BDUND electrodes in solution of )185 ( )]TJ -0.0004 Tc 0.0029 Tw -20.38 -1.15 Td [(50 mm)7.4 (ol L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 143.28 505.08 Tm (-1)Tj 0 Tc 12 0 0 12 150 499.56 Tm ( H)Tj 7.98 0 0 7.98 161.64 498.06 Tm (2)Tj -0.00121 Tc 12 0 0 12 165.66 499.56 Tm (SO)Tj 0 Tc 7.98 0 0 7.98 180.96 498.06 Tm (4)Tj 0.00011 Tc 0.0007 Tw 12 0 0 12 184.98 499.56 Tm [( support electrolyte containing 1 mm)7.9 (ol L)]TJ 0.00529 Tc 0 Tw 7.98 0 0 7.98 381.6 505.08 Tm (-1)Tj -0.0009 Tc 0.0009 Tw 12 0 0 12 388.32 499.56 Tm ( CuSO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 420.6 498.06 Tm (4)Tj 12 0 0 12 424.62 499.56 Tm (. )Tj -26.395 -1.15 Td ( )Tj 0.0004 Tc 0.0746 Tw 0 -1.15 TD [(The processes of deposition and dissolution )6.1 (are clear for both film)8.1 (s. However, thes)4.5 (e )]TJ 0.0006 Tc 0.0094 Tw -1.49 -1.15 Td [(results were influenced by the film)8.4 ( morphol)]TJ 0 Tc 0.00999 Tw 17.62 0 Td (ogies. The potential sweep)Tj 0.0005 Tc 0.00951 Tw (ing started at 0.7 V )Tj 0.00011 Tc 0.0699 Tw -17.62 -1.15 Td (and during the negative potential scan two Cu)Tj 0.0006 Tc 0.0685 Tw 18.85 0 Td [( ca)-5.6 (thodic current peaks were observed for )]TJ 0.0005 Tc 0.0936 Tw -18.85 -1.15 Td (BDD electrode. The first cathodic current peak)Tj 0.0006 Tc 0.09441 Tw 19.375 0 Td [(, at around -0.4 V, m)8.4 (a)-0.6 (y be associated to )]TJ -0.0005 Tc 0.0455 Tw -19.375 -1.145 Td (the reduction of Cu)Tj 0.0038 Tc 0 Tw 7.98 0 0 7.98 184.5 422.34 Tm (2+)Tj -0.0005 Tc 0.0455 Tw 12 0 0 12 193.02 416.82 Tm ( to Cu)Tj 0 Tc 0 Tw 7.98 0 0 7.98 223.44 422.34 Tm (+)Tj -0.00011 Tc 0.0451 Tw 12 0 0 12 227.94 416.82 Tm [( ions. T)5.7 (h)-0.1 (e second peak, at around -0.6 V, corresponds to the )]TJ -0.002 Tc 0 Tw -11.495 -1.15 Td (Cu)Tj 0 Tc 7.98 0 0 7.98 103.98 408.54 Tm (+)Tj 0.00079 Tc 0.1037 Tw 12 0 0 12 108.48 403.02 Tm [( ions to)5.8 ( the m)8.6 (e)-0.4 (tallic)4.6 ( Cu or d)5.8 (i)-1.4 (re)4.6 (c)4.6 (tly f)3.8 (r)-1.2 (om)8.6 ( the)4.6 ( Cu)]TJ 0.0038 Tc 0 Tw 7.98 0 0 7.98 346.08 408.54 Tm (2+)Tj 0.0005 Tc 0.10361 Tw 12 0 0 12 354.6 403.02 Tm [( ions)4.7 ( to the)4.3 ( m)8.3 (e)-0.7 (tallic Cu reduc)4.3 (tion )]TJ 0.00031 Tc 0.2063 Tw -22.05 -1.15 Td (process. In the reverse potential scan, two )Tj 0.0007 Tc 0.2093 Tw 18.43 0 Td [(cro)5.7 (sses were o)5.7 (b)0.7 (served according to)5.7 ( th)5.7 (ose )]TJ 0.0005 Tc -0.00301 Tw -18.43 -1.15 Td (observed by Fletcher )Tj /TT4 1 Tf 0.0011 Tc -0.0011 Tw 8.64 0 Td [(et a)6.1 (l)-1.1 (.)]TJ /TT2 1 Tf 0.00031 Tc -0.0013 Tw 2 0 Td ( \(13\). The more cathodic crossing )Tj 0.00011 Tc -0.00011 Tw [-0.4 (at -0.37 V is characterized as )]TJ 0.0005 Tc 0.2395 Tw -10.64 -1.15 Td (the nucleation \(E)Tj 0 Tc 0 Tw 7.98 0 0 7.98 177.78 360.12 Tm (n)Tj 0.00031 Tc 0.2397 Tw 12 0 0 12 181.8 361.62 Tm (\), whereas the second crossing at )Tj 0.0002 Tc 0.23981 Tw 14.86 0 Td (-0.06 V indicates the reversible )Tj 0.0009 Tc 0.0341 Tw -22.51 -1.15 Td (potential \(E)Tj -0.0097 Tc 0 Tw 7.98 0 0 7.98 146.82 346.32 Tm [(re)-9.5 (v)]TJ 0.0002 Tc 0.03481 Tw 12 0 0 12 156.96 347.82 Tm (\) of the Cu)Tj 0.0038 Tc 0 Tw 7.98 0 0 7.98 209.94 353.34 Tm (2+)Tj 0.0007 Tc 0.0363 Tw 12 0 0 12 218.46 347.82 Tm [(/Cu syste)4.5 (m)3.5 (. In m)8.5 (o)0.7 (re positiv)5.7 (e poten)]TJ 0.00121 Tc 0.0338 Tw 14.18 0 Td [(tia)5 (ls, the a)5 (ppearanc)5 (e of)4.2 ( two )]TJ 0.00011 Tc 0.0593 Tw -24.885 -1.15 Td (anodic current peaks at 0.15 V and at 0.30 V )Tj 0.0002 Tc 0.05811 Tw [-0.2 (indicates the Cu di)]TJ 0.00011 Tc 0.05991 Tw (ssolution corresponding )Tj 0.0002 Tc -0.0002 Tw T* (to the different Cu phases deposited duri)Tj 0.0009 Tc -0.0016 Tw 16.225 0 Td [(ng the n)5.9 (e)-0.3 (gativ)5.9 (e pote)4.7 (n)0.9 (tia)4.7 (l sweep. For the BDUND )]TJ 0.00011 Tc 0.0289 Tw -16.225 -1.15 Td (electrode, the behavior is a li)Tj 0.0009 Tc 0.0284 Tw 11.7 0 Td [(ttle)4.7 ( dif)3.9 (f)3.9 (e)-0.3 (rent.)5.9 ( Durin)5.9 (g)0.9 ( the s)5.1 (can to)5.9 (ward negative poten)5.9 (tia)4.7 (ls)5.1 ( the )]TJ 0.0006 Tc 0.10851 Tw -11.7 -1.15 Td (cathodic current started to increase at ar)Tj 0.10941 Tw 16.61 0 Td [(ound -0)5.6 (.23 V indicating that th)5.6 (e Cu deposition )]TJ 0.00439 Tw -16.61 -1.15 Td (process began at this potentia)Tj 0.0004 Tc 0.0036 Tw 11.8 0 Td (l. The two Cu reduction processe)Tj 0.00459 Tw 13.24 0 Td (s were not clearly observed, )Tj 0.00079 Tc 0.00841 Tw -25.04 -1.15 Td (as noted in the BDD electrode. This behavior )Tj 0.0005 Tc 0.00951 Tw 18.455 0 Td [(m)8.3 (a)-0.7 (y be attributed to a less favorable energy )]TJ -0.00031 Tc 0.05029 Tw -18.455 -1.15 Td (condition for the Cu)Tj 0.0038 Tc 0 Tw 7.98 0 0 7.98 188.76 256.7401 Tm (2+)Tj 0.00011 Tc 0.04739 Tw 12 0 0 12 197.28 251.22 Tm [( to)5.1 ( Cu)]TJ 0 Tc 0 Tw 7.98 0 0 7.98 227.7 256.7401 Tm (+)Tj 0.00011 Tc 0.0479 Tw 12 0 0 12 232.2 251.22 Tm ( ions reduction process on th)Tj 0 Tc 0.05 Tw 11.715 0 Td [(e BDUND. Leading th)5 (e sw)7.2 (eep )]TJ 0.0002 Tc 0.0298 Tw -23.565 -1.15 Td (reversal at -0.9 V, two crosses were also )Tj 0 Tc 0.03 Tw 16.63 0 Td (observed at -0.25 and -0.08 V, corresponding to )Tj 0.0009 Tc 0.05409 Tw -16.63 -1.15 Td [(the nucle)4.7 (ation and the reversib)5.9 (le po)5.9 (tentials, )]TJ 0.00101 Tc 0.05299 Tw 17.98 0 Td [(r)4 (e)-0.2 (sp)6 (ectiv)6 (ely. In more positiv)6 (e potentials,)6 ( the)4.8 ( )]TJ 0.0005 Tc 0.022 Tw -17.98 -1.15 Td (appearance of a peak cu)Tj -0.0002 Tc 0.02431 Tw 9.695 0 Td (rrent at 0.12 V indicates the bulk )Tj 0.00031 Tc 0.0222 Tw [0.2 (Cu stripping. B)7.3 (e)-0.9 (si)]TJ 0 Tc 0.02251 Tw [-0.5 (des, this peak )]TJ 0.0005 Tc 0.13451 Tw -9.695 -1.15 Td (is followed by a slight shoulder of anodic cu)Tj 0.00011 Tc 0.1349 Tw 18.87 0 Td [(rrent concerning a sm)7.9 (all amount of other )]TJ 0.0004 Tc 0.00459 Tw -18.87 -1.15 Td (electrodeposited Cu phases. Considering the Cu)Tj 0.00079 Tc 0.0029 Tw 19.195 0 Td [( electrochem)8.6 (ical pro)5.8 (cess presented ab)5.8 (ove,)5.8 ( )]TJ 0.0004 Tc -0.0004 Tw -19.195 -1.15 Td [(the optim)8.2 (um potential for the photoelectrode)]TJ 0 Tc 0 Tw 17.92 0 Td (position was found at -0.6 V, which certainly )Tj 0.00121 Tc -0.00191 Tw -17.92 -1.15 Td [(perm)9 (itted to contro)6.2 (l the d)6.2 (eposits f)4.2 (o)1.2 (r b)6.2 (o)1.2 (th ele)5 (ctrod)6.2 (es. )]TJ 0 Tc 0 Tw T* ( )Tj 0.0002 Tc -0.0002 Tw T* (Copper particles photoelectrodeposition and nitrate reduction)Tj ET 90 125.1 294.24 0.60001 re f BT /TT2 1 Tf 0 Tc 0 Tw 12 0 0 12 384.24 127.0201 Tm ( )Tj -24.52 -1.15 Td ( )Tj 0.00011 Tc 0.59399 Tw 1.49 -1.15 Td (Figure 2 shows the SEM images of)Tj 0.00031 Tc 0.5947 Tw 17.62 0 Td [( th)5.3 (e diam)8.1 (ond surface after the Cu )]TJ 0.0007 Tc 0.013 Tw -19.11 -1.15 Td [(photoelectrodeposition, where im)8.5 (ages \(a\) and )]TJ 0 Tc 0.015 Tw 18.575 0 Td (\(b\) refer to the BDD )Tj 0.00031 Tc 0.0163 Tw 8.485 0 Td (and the BDUND film, )Tj 0.0007 Tc 0.2493 Tw -27.06 -1.15 Td [(respec)4.5 (tive)4.5 (l)-1.5 (y.)5.7 ( Figure 2)5.7 ( s)4.9 (hows the s)4.9 (u)0.7 (rface m)8.5 (odification)5.7 ( of Cu particle)4.5 (s)4.9 ( resu)5.7 (lting)5.7 ( in a )]TJ 0.00031 Tc -0.00031 Tw T* [(morphology com)8.1 (posed of rounded grains distribu)]TJ 0.0002 Tc -0.0002 Tw 19.805 0 Td (ted throughout the surf)Tj 0.0004 Tc 0.00079 Tw 9.135 0 Td [(ace of both film)8.2 (s. )]TJ ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 298.5 12 Td (179)Tj ET Q BT /GS1 gs /T1_1 1 Tf 0 Tc 0 Tw 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_1 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_1 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 85 0 obj <> endobj 110 0 obj <> endobj 111 0 obj <> endobj 112 0 obj <> endobj 80 0 obj [113 0 R 114 0 R] endobj 81 0 obj <>stream BT /GS0 gs /TT0 1 Tf 0.1825 Tw 12 0 0 12 90 726.84 Tm (potential \(-4.0 V )Tj /TT1 1 Tf 0.00079 Tc 0 Tw 7.44 0 Td (versus)Tj /TT0 1 Tf 0.00011 Tc 0.18491 Tw [-0.2 ( SHE\), the photogenerated electrons in diam)7.9 (ond surface have)-6 ( )]TJ 0.0005 Tc -0.00169 Tw -7.44 -1.15 Td [(extrem)8.3 (ely high reducing power. Nevertheless,)]TJ 0.0004 Tc -0.0016 Tw 18.445 0 Td ( after the boron doping, )Tj 0.00011 Tc -0.00259 Tw 9.665 0 Td [(the BDD electrodes)-5.7 ( )]TJ 0.00101 Tc 0.067 Tw -28.11 -1.15 Td [(present the Ferm)8.8 (i level at ar)]TJ 0.00011 Tc 0.0699 Tw 11.545 0 Td [(ound 0.4 eV from)7.9 ( the top of )]TJ -0.00011 Tc 0.0701 Tw 11.92 0 Td (the valence band and works as )Tj 0.0005 Tc 0.07381 Tw -23.465 -1.15 Td [(the boron acceptor level \(11\). So, the diam)8.3 (ond se)]TJ 0.0009 Tc 0.0741 Tw [-0.2 (rves as a so)5.9 (urce of electrons to redu)5.9 (ce )]TJ 0.0002 Tc -0.0016 Tw 0 -1.15 TD (the ions to be deposited as well as)Tj -0.00011 Tc -0.00191 Tw 13.585 0 Td ( a substrate for their deposition. )Tj 0.0004 Tc 0.34019 Tw -13.585 -1.15 Td [(Thus, the aim)8.2 ( of this work is to m)8.2 (a)]TJ 0.0006 Tc 0.3385 Tw 16.69 0 Td [(ke a com)8.4 (p)0.6 (arative study betw)7.8 (een the copper )]TJ 0.00031 Tc 0.2159 Tw -16.69 -1.15 Td [(photoelectrodeposition onto boron doped m)8.1 (i)-1.9 (cr)]TJ 0 Tc 0.2162 Tw 19.42 0 Td [(ocrystalline diam)7.8 (ond \()-7 (B)2 (DD\) and boron )]TJ 0.42 Tw -19.42 -1.15 Td [(doped ultra-nanocrystalline diam)7.8 (ond \(BDUND\))]TJ 0.0006 Tc 0.4194 Tw 20.445 0 Td [(. W)9.4 (e)-0.6 ( discuss the influence of the)-5.5 ( )]TJ 0.00079 Tc 0.0237 Tw -20.445 -1.15 Td [(morphology, the crystal size, th)5.8 (e cry)5.8 (stallograph)5.8 (i)3.6 (c orien)5.8 (t)-1.4 (ation)5.8 (,)0.8 ( and the surface term)8.6 (ination )]TJ -0.0004 Tc 0.1754 Tw T* (in the reactivities of photoge)Tj 0.0002 Tc 0.1731 Tw 12.135 0 Td (nerated electrons to understa)Tj 0.00011 Tc 0.1732 Tw 11.99 0 Td (nd the copper photocatalytic )Tj 0.0007 Tc 0.423 Tw -24.125 -1.15 Td [(deposition in diam)8.5 (ond film)8.5 (s. Furtherm)8.5 (ore,)]TJ 0 Tc 0.425 Tw 18.69 0 Td [( the electrochem)7.8 (i)-2.2 (cal response of these)-6.1 ( )]TJ 0.0005 Tc -0.00211 Tw -18.69 -1.15 Td (modified electrodes was studied )Tj 0.00011 Tc -0.00169 Tw 13.115 0 Td (for nitrate electroreduction. )Tj 0 Tc 0 Tw -13.115 -1.15 Td ( )Tj /TT2 1 Tf 0.00011 Tc -0.00011 Tw 12.735 -1.16 Td (Experimental Procedure )Tj /TT0 1 Tf 0 Tc 0 Tw -12.735 -1.14 Td ( )Tj 0.0006 Tc 0.0744 Tw 1.49 -1.15 Td [(The film)8.4 (s were grown by hot filam)8.4 (e)-0.6 (nt-ass)]TJ 0.00011 Tc 0.07491 Tw 17.22 0 Td [(isted chem)7.9 (ical vapor deposition \(HFCVD\) )]TJ 0 Tc 0.075 Tw -18.71 -1.15 Td [(technique using the following growth param)7.8 (e)-1.2 (ters: 800 )]TJ 0 Tw 7.98 0 0 7.98 359.16 511.56 Tm (o)Tj -0.00011 Tc 0.0751 Tw 12 0 0 12 363.18 506.04 Tm [(C, 50 Torr, 16 h, gas m)7.7 (i)-2.3 (xture of )]TJ 0.0005 Tc 0.53951 Tw -22.765 -1.15 Td [(1/99 % of)8.5 ( the CH)]TJ 0 Tc 0 Tw 7.98 0 0 7.98 200.52 490.7401 Tm (4)Tj -0.00281 Tc 12 0 0 12 204.54 492.2401 Tm (/H)Tj 0 Tc 7.98 0 0 7.98 216.48 490.7401 Tm (2)Tj -0.0004 Tc 0.54041 Tw 12 0 0 12 220.5 492.2401 Tm ( for BDD and 650 )Tj 0 Tc 0 Tw 7.98 0 0 7.98 342.48 497.76 Tm (o)Tj 0.0002 Tc 0.53889 Tw 12 0 0 12 346.5 492.2401 Tm [(C, 30 Torr 16 h, gas m)8 (i)-2 (xture)-6 ( )539.1 ( )]TJ 0.0004 Tc 0.14861 Tw -21.375 -1.15 Td [(of 1/19/80 % of the C)7.4 (H)]TJ 0 Tc 0 Tw 7.98 0 0 7.98 211.86 476.94 Tm (4)Tj 0.0022 Tc 12 0 0 12 215.88 478.44 Tm (/H)Tj 0 Tc 7.98 0 0 7.98 227.88 476.94 Tm (2)Tj 0.00011 Tc 0.15089 Tw 12 0 0 12 231.9 478.44 Tm [(/Ar for BDUND. The film)7.9 (s we)]TJ 0.0002 Tc 0.1498 Tw 13.075 0 Td (re deposited on the silicon )Tj 0.0009 Tc 0.36909 Tw -24.9 -1.15 Td [(substrate af)8.9 (ter s)5.1 (eeding)5.9 ( pre-treatment \(1)]TJ 0 Tc 17.145 0 Td (2\). The boron source was obtained by an )Tj -0.0004 Tc 0.37869 Tw -17.145 -1.15 Td (additional hydrogen line passing )Tj 0.38029 Tw 14.785 0 Td (through a bubbler containing B)Tj 0 Tc 0 Tw 7.98 0 0 7.98 435.48 449.34 Tm (2)Tj 12 0 0 12 439.5 450.84 Tm (O)Tj 7.98 0 0 7.98 448.14 449.34 Tm (3)Tj 0.0016 Tc 0.3784 Tw 12 0 0 12 452.16 450.84 Tm [( disso)6.6 (lv)6.6 (ed in )]TJ 0.0005 Tc 0.1145 Tw -30.18 -1.15 Td [(m)8.3 (e)-0.7 (thanol. The doping level co)5.5 (rresp)5.5 (onds )]TJ 0.1136 Tw 16.9 0 Td [(to th)5.5 (e accepto)5.5 (r densities of around 10)]TJ 0.0038 Tc 0 Tw 7.98 0 0 7.98 480.96 442.56 Tm (21)Tj -0.0033 Tc 0.1183 Tw 12 0 0 12 489 437.04 Tm [( ato)-8.3 (m)4.5 (s)-9.1 ( )]TJ 0.00121 Tc 0 Tw -33.25 -1.15 Td (cm)Tj -0.0022 Tc 7.98 0 0 7.98 104.64 428.76 Tm (-3)Tj 0.00079 Tc -0.00011 Tw 12 0 0 12 111.3 423.24 Tm [( estim)8.6 (ated from)8.6 ( Ra)-5.4 (m)8.6 (a)-0.4 (n')6 (s measurem)8.6 (ents \(not shown\). )]TJ 0.0009 Tc 0.5141 Tw -0.285 -1.15 Td [(The electro)5.9 (chem)8.7 (ical m)8.7 (easurem)8.7 (ents were made using Autolab PGSTAT 302)5.9 ( )]TJ 0.0004 Tc 0.0096 Tw -1.49 -1.15 Td [(equipm)8.2 (ent with a three-electr)]TJ 0.0005 Tc 0.0085 Tw 11.775 0 Td (ode cell. The geometric area of)Tj 0.0007 Tc 0.00929 Tw 12.485 0 Td [( the diam)8.5 (ond film)8.5 (s in contact )]TJ -0.0004 Tc 0.1304 Tw -24.26 -1.15 Td (with the electrolyte was 0.13 cm)Tj 0 Tc 0 Tw 7.98 0 0 7.98 253.56 387.36 Tm (2)Tj 0.0002 Tc 0.131 Tw 12 0 0 12 257.58 381.84 Tm [(. A platinum)8 ( m)8 (e)-1 (sh served )]TJ 0.1273 Tw 11.145 0 Td [(as a coun)5.2 (ter electrode and )]TJ -0.0005 Tc 0 Tw -25.11 -1.15 Td (Ag/AgCl/KCl)Tj -0.00011 Tc 7.98 0 0 7.98 157.32 366.54 Tm (\(sat\))Tj 0.0005 Tc 0.06531 Tw 12 0 0 12 171.48 368.04 Tm ( was used as the reference electrode. )Tj 0.0013 Tc 0.0627 Tw 15.3 0 Td [(All e)5.1 (l)4.1 (ectrod)6.3 (e)0.1 ( pote)5.1 (n)1.3 (tia)5.1 (ls in the text )]TJ 0.0006 Tc 0.19099 Tw -22.09 -1.15 Td (are referred to this)Tj -0.0005 Tc 0.1955 Tw 7.935 0 Td ( electrode. The photoelectrodepositi)Tj 0.0002 Tc 0.1938 Tw 14.96 0 Td (on of Cu particles on diamond )Tj 0.0004 Tc 0.03461 Tw -22.895 -1.15 Td [(film)8.2 (s was perform)8.2 (e)-0.8 (d in the potentiostatic m)8.2 (ode)]TJ -0.0004 Tc 0.0354 Tw 19.085 0 Td [(, at a fixed potential of -0.6 V for 10 m)7.4 (i)-2.6 (n, )]TJ -0.00011 Tc 0.02631 Tw -19.085 -1.15 Td [(in a 1 mm)7.7 (ol)-7.3 ( L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 159.24 332.16 Tm (-1)Tj -0.00101 Tc 0.026 Tw 12 0 0 12 165.9 326.64 Tm [( CuS)-4.8 (O)]TJ 0 Tc 0 Tw 7.98 0 0 7.98 198.54 325.14 Tm (4)Tj -0.0004 Tc 0.0287 Tw 12 0 0 12 202.56 326.64 Tm [(, 50 mm)7.4 (ol L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 262.86 332.16 Tm (-1)Tj 0.02499 Tc 12 0 0 12 269.52 326.64 Tm ( H)Tj 0 Tc 7.98 0 0 7.98 281.46 325.14 Tm (2)Tj -0.00121 Tc 12 0 0 12 285.48 326.64 Tm (SO)Tj 0 Tc 7.98 0 0 7.98 300.78 325.14 Tm (4)Tj 0.00031 Tc 0.0247 Tw 12 0 0 12 304.8 326.64 Tm ( aqueous solution, under UV irradiation. The )Tj 0.1947 Tw -17.9 -1.15 Td [(light source was a hom)8.1 (e m)8.1 (a)-0.9 (de system)8.1 (, com)8.1 (pos)]TJ 0.0007 Tc 0.1935 Tw [-0.5 (ed of a set of five comm)8.5 (ercial lam)8.5 (p)0.7 (s )]TJ 0.08501 Tw T* [(\(Philip)5.7 (s TUV 30 W)9.5 (/)-6.5 (G30T8\) placed)5.7 ( in a closed)]TJ 0.0004 Tc 0.08459 Tw 19.295 0 Td [( box. The UV irradian)5.4 (ce at the electrode )]TJ 0.0006 Tc 0.28439 Tw -19.295 -1.15 Td [(position)5.6 ( was 12 W)9.4 (/)-6.6 (m)]TJ 0.01131 Tc 0 Tw 7.98 0 0 7.98 202.5 290.7601 Tm (2 )Tj 0.0005 Tc 0.2832 Tw 12 0 0 12 211.44 285.2401 Tm [(m)8.3 (easured by a rad)5.5 (i)-1.7 (o)5.5 (m)8.3 (eter. Befo)]TJ 0.00031 Tc 0.2847 Tw 13.93 0 Td [(re \(30 m)8.1 (i)-1.9 (n\) and during the )]TJ 0.00011 Tc 0.15401 Tw -24.05 -1.15 Td (photoelectrodeposition, the solution was purged with N)Tj 0 Tc 0 Tw 7.98 0 0 7.98 367.44 269.9401 Tm (2)Tj 0.155 Tw 12 0 0 12 371.46 271.4401 Tm [(. The m)7.8 (orphologies of the Cu )]TJ 0.00011 Tc 0.19591 Tw -23.455 -1.15 Td [(modified diam)7.9 (ond fil)-7.1 (m)2.9 (s were verified fr)]TJ 0.0006 Tc 0.19341 Tw 17.115 0 Td [(om)8.4 ( the scanning electron m)8.4 (i)-1.6 (croscopy \(S)6.8 (EM\) )]TJ 0.00079 Tc 0.2692 Tw -17.115 -1.15 Td [(im)8.6 (ages using a Jeol JS)7 (M-5310 m)8.6 (i)-6.4 (croscope. )]TJ 0.0006 Tc 0.26691 Tw 19.21 0 Td [(T)6.4 (h)0.6 (e nitrate reduction experim)8.4 (e)-0.6 (nts were )]TJ 0.0002 Tc 0.11349 Tw -19.21 -1.15 Td (monitored by the linear sw)Tj 0 Tc 0.11501 Tw 11.175 0 Td [(eep voltammetry using 0.01 m)7.8 (ol)-7.2 ( L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 396.96 235.5601 Tm (-1)Tj 0.1172 Tw 12 0 0 12 403.62 230.0401 Tm ( KNO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 433.92 228.5401 Tm (3)Tj 0.00031 Tc 0.11591 Tw 12 0 0 12 437.94 230.0401 Tm [( + 0.001 m)8.1 (o)0.3 (l)-6.9 ( L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 515.28 235.5601 Tm (-1)Tj 0 Tc 12 0 0 12 521.9999 230.0401 Tm ( )Tj 0.00031 Tc -0.00031 Tw -36 -1.15 Td [(Britton)5.3 (-)-1.7 (Robinson \(BR\) buf)3.3 (f)3.3 (e)-0.9 (r \(pH=3\). )]TJ 0 Tc 0 Tw T* ( )Tj /TT2 1 Tf 0.00031 Tc -0.00031 Tw 13.22 -1.16 Td [(Results and discussion)6.5 ( )]TJ 0 Tc 0 Tw 4.78 -1.15 Td ( )Tj /TT0 1 Tf 0.0004 Tc -0.002 Tw -18 -1.14 Td [(Electrochemical responses of diam)8.2 (o)]TJ -0.00031 Tw 14.47 0 Td [(nd film)8.1 (s in the cooper electrodeposition)]TJ ET 90 159.12 364.56 0.59999 re f BT /TT1 1 Tf 0 Tc 0 Tw 12 0 0 12 454.56 161.0401 Tm ( )Tj /TT0 1 Tf -30.38 -1.725 Td ( )Tj -0.0004 Tc 0.01041 Tw 1.49 -1.15 Td [(Firstly, a cyclic voltamm)7.4 (etry at 100 mV s)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 308.52 132.0601 Tm (-1)Tj 0.0004 Tc 0.0083 Tw 12 0 0 12 315.18 126.54 Tm [( was perform)8.2 (e)-0.8 (d in orde)]TJ 0.0096 Tw 9.305 0 Td [(r to)5.4 ( ch)5.4 (aracterize th)5.4 (e )]TJ 0.2596 Tw -28.07 -1.15 Td [(Cu reductio)5.4 (n and oxidation processes on )]TJ -0.0002 Tc 0.261 Tw 18.065 0 Td [(the BDD and the BDUND surfaces. Thi)-7.4 (s)-6 ( )]TJ 0.00011 Tc 0.3799 Tw -18.065 -1.15 Td [(procedure is im)7.9 (portant to choose the suit)]TJ -0.00031 Tc 0.38029 Tw 18.555 0 Td (able potential to be)Tj 0.3804 Tw 8.775 0 Td [( applied during the)-6.6 ( )]TJ 0.0002 Tc 0.2998 Tw -27.33 -1.15 Td (photoelectrodeposition. Figur)Tj -0.00031 Tc 0.3047 Tw 12.14 0 Td [(e 1 shows cyclic voltamm)7.5 (ogr)-7.3 (am)7.5 (s of Cu on BDD and )]TJ 0.0006 Tc 0.0006 Tw -12.14 -1.15 Td [(BDUND f)3.6 (ilm)8.4 (s in a soluti)]TJ 0 Tc 0.0025 Tw [0.1 (on containing 1 mm)7.8 (ol L)]TJ -0.0022 Tc 0 Tw 7.98 0 0 7.98 326.7 76.86 Tm (-1)Tj -0.0009 Tc 0.0009 Tw 12 0 0 12 333.36 71.3401 Tm ( CuSO)Tj 0 Tc 0 Tw 7.98 0 0 7.98 365.64 69.8401 Tm (4)Tj -0.0004 Tc 0.0016 Tw 12 0 0 12 369.66 71.3401 Tm [( +)-6.4 ( 50 mm)7.4 (ol L)]TJ 0.00529 Tc 0 Tw 7.98 0 0 7.98 435.78 76.86 Tm (-1)Tj 0 Tc 12 0 0 12 442.5 71.3401 Tm ( H)Tj 7.98 0 0 7.98 454.14 69.8401 Tm (2)Tj -0.00121 Tc 12 0 0 12 458.16 71.3401 Tm (SO)Tj 0 Tc 7.98 0 0 7.98 473.46 69.8401 Tm (4)Tj 12 0 0 12 477.48 71.3401 Tm (. )Tj -30.8 -1.15 Td ( )Tj ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 298.5 12 Td (178)Tj ET Q BT /GS1 gs /T1_1 1 Tf 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_1 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_1 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 82 0 obj <> endobj 113 0 obj <> endobj 114 0 obj <> endobj 115 0 obj <> endobj 75 0 obj [116 0 R 117 0 R] endobj 76 0 obj <>stream BT /GS0 gs /TT0 1 Tf 0.0004 Tc -0.0004 Tw 12 0 0 12 93.12 726.72 Tm [(Copper Photoele)4.2 (ctrod)6.6 (e)-0.8 (position o)5.4 (n)1.6 (to Boron Doped Micro and Ultra-nanocryst)3.4 (alline )]TJ 0.00011 Tc -0.00011 Tw 5.645 -1.15 Td [(Diamond Electrodes Applied to Nitrate Electroreduction)6.3 ( )]TJ /TT1 1 Tf 0 Tc 0 Tw -4.405 -1.14 Td ( )Tj -0.0002 Tc 0.0002 Tw 8.08 -1.15 Td [(A. B. Couto, M. R. Baldan, N. G. Fe)-6.4 (rreira )]TJ 0 Tc 0 Tw 8.42 -1.15 Td ( )Tj 0.0002 Tc -0.0002 Tw -14.415 -1.15 Td (Instituto Nacional de Pesquisas Espaci)Tj 0 Tc 0 Tw 15.445 0 Td [(ais, S\343o Jos\351 dos Cam)7.8 (p)-5 (os, Brasil. )]TJ -1.03 -1.15 Td ( )Tj 0 -1.15 TD ( )Tj 0.0002 Tc 0.1048 Tw -13.5 -1.15 Td (The influence of the boron doped )Tj 0.0004 Tc 0.1046 Tw 14.235 0 Td [(m)8.2 (i)-1.8 (cro and ultra-nanocrystalline )]TJ 0.0002 Tc 0.53551 Tw -14.235 -1.15 Td [(diam)8 (ond \()-6.8 (B)2.2 (DD and BDUND\))-6.8 ( m)8 (o)0.2 (rphologies in the copper )]TJ 0.00011 Tc 0.3324 Tw T* (photoelectrodeposition was investig)Tj 0.3349 Tw 15.055 0 Td (ated. Copper particles were )Tj 0.0004 Tc 0.1696 Tw -15.055 -1.15 Td (deposited in the potentiostat m)Tj 0.00011 Tc 0.1689 Tw 12.955 0 Td [(ode and under UV irradiation for)-6.9 ( )]TJ 0.0006 Tc 0.2894 Tw -12.955 -1.15 Td [(both electro)5.6 (d)0.6 (es. For BDD, the )]TJ 0.00031 Tc 0.2897 Tw 13.76 0 Td (copper deposits presented high )Tj 0.0015 Tc 0.2075 Tw -13.76 -1.15 Td [(density and)6.5 ( unif)4.5 (o)1.5 (rm)9.3 (ity all over th)]TJ 0.00011 Tc 0.2099 Tw 14.47 0 Td (e crystal faces. This behavior )Tj 0.2039 Tw -14.47 -1.15 Td [(m)7.9 (a)-1.1 (y be explained by its sem)7.9 (i)-2.1 (conduc)]TJ -0.0006 Tc 0.2056 Tw 15.54 0 Td (tor character that promoted )Tj 0.0004 Tc 0.7821 Tw -15.54 -1.15 Td (additional photogenerated elect)Tj 0.0002 Tc 0.78481 Tw 14.12 0 Td (rons enhancing the copper )Tj 0.0004 Tc 0.22459 Tw -14.12 -1.15 Td (reduction reaction. Otherwise, for BDUND the copper particles )Tj 0.0005 Tc 0.18449 Tw T* [(were rando)5.5 (m)8.3 (l)-1.7 (y located with low )]TJ 0.00011 Tc 0.1815 Tw 14.12 0 Td (density. Concerning the nitrate )Tj -0.00031 Tc 0.45531 Tw -14.12 -1.15 Td [(reduction process, Cu/BDD pres)-0.2 (ented a better response and )]TJ 0.0002 Tc -0.0002 Tw T* [(reproducibility com)8 (p)0.2 (ared to those for the Cu/BDUND electrode. )]TJ 0 Tc 0 Tw T* ( )Tj /TT0 1 Tf 0.0005 Tc -0.0005 Tw 10.775 -1.16 Td [(Introductio)5.5 (n)1.7 ( )]TJ 0 Tc 0 Tw 2.725 -1.15 Td ( )Tj /TT1 1 Tf 0.0011 Tc 0.07719 Tw -18 -1.14 Td [(Nitrate has been consid)6.1 (ered an im)8.9 (portan)6.1 (t e)]TJ 0.07899 Tw 17.59 0 Td [(nvir)4 (o)1 (nm)8.8 (ental co)6 (ntam)8.8 (inant of)4 ( soil and n)6 (a)-0.2 (tur)4 (a)4.8 (l )]TJ 0.019 Tw -17.59 -1.15 Td [(waters \(grou)6 (nd and surface water\). T)6.8 (h)1 (is contam)8.8 (ination is m)8.8 (a)-0.2 (inly due to the excessiv)6 (e)4.8 ( use )]TJ 0.00079 Tc 0.0482 Tw T* [(of nitrogen)5.8 ( fertilizers)5 ( in the so)5.8 (il,)]TJ 0.0011 Tc 0.0459 Tw 13.19 0 Td [( esp)6.1 (ecially in ru)6.1 (ral and ag)6.1 (ri)]TJ 0.0004 Tc 0.04961 Tw 11.155 0 Td [(cultural areas)4.6 (.)0.4 ( Because of)8.4 ( its)4.6 ( )]TJ 0.0007 Tc 0.03349 Tw -24.345 -1.15 Td [(high m)8.5 (obility, the irrig)5.7 (a)-0.5 (tion proce)4.5 (ss and the r)3.7 (a)-0.5 (in)]TJ 0.00079 Tc 0.0334 Tw 19.575 0 Td [( water a)4.6 (r)-1.2 (e ca)4.6 (pable of)3.8 ( car)3.8 (rying th)5.8 (e nitrate)4.6 ( )]TJ 0 Tc 0.1593 Tw -19.575 -1.15 Td (not only on the surface but it also penetrat)Tj 0.0007 Tc 0.1584 Tw [0.4 (es)4.9 ( the soil,)5.7 ( thu)5.7 (s)-0.1 ( contam)8.5 (inating large areas. )]TJ 0.00011 Tc 0.1899 Tw T* [(Consequently, m)7.9 (a)-1.1 (ny studies have appeared )4.1 (over the re)4 (cent years)4.3 ( in)5.1 ( which researches)4.3 ( )]TJ 0.0005 Tc -0.0005 Tw T* [(attem)8.3 (p)0.5 (t to convert nitrate )]TJ 0.0004 Tc -0.002 Tw 10.33 0 Td [(into harm)8.2 (less nitrogen \(1\). )]TJ 0.00011 Tc 0.26489 Tw -10.33 -1.15 Td [(Nitrate electroreduction is one of the m)7.9 (e)-1.1 (t)]TJ 0.0002 Tc 0.26401 Tw 18.02 0 Td [(hods used to rem)8 (ove these ions from)8 ( the )]TJ 0.00031 Tc 0.0347 Tw -18.02 -1.15 Td [(polluted waters. Thus, the electrochem)8.1 (i)-1.9 (cal pro)]TJ 0.0006 Tc 0.0336 Tw 18.7 0 Td [(ces)4.8 (s appears to be a clean, h)5.6 (i)-1.6 (ghly effective )]TJ 0.0004 Tc 0.0146 Tw -18.7 -1.15 Td (and inexpensive alternative te)Tj 0.0134 Tw 11.96 0 Td (chnique \(2\). In this sense,)Tj -0.00031 Tc 0.0153 Tw 10.335 0 Td ( boron doped diamond \(BDD\) has )Tj 0.0004 Tc 0.2646 Tw -22.295 -1.15 Td [(been reported to)5.4 ( be an excellen)5.4 (t)3.2 ( electrod)5.4 (e )]TJ -0.0004 Tc 0.2654 Tw 18.75 0 Td (to study the nitrate )Tj 0.00079 Tc 0.2625 Tw [0.2 (r)3.8 (e)-0.4 (d)5.8 (u)0.8 (ction)5.8 ( due to its)5 ( )]TJ 0.00031 Tc 0.24471 Tw -18.75 -1.15 Td [(outstanding electrochem)8.1 (ical features such )]TJ 0 Tc 0.24409 Tw [-0.5 (as: the wide potential window in aqueous )]TJ 0.00079 Tc 0.0984 Tw T* [(solution)5.8 (s an)5.8 (d the)4.6 ( weak adsorption f)8.8 (o)0.8 (r m)8.6 (o)0.8 (st ty)]TJ -0.0002 Tc 0.09891 Tw 18.935 0 Td [(pes of m)7.6 (o)-0.2 (lecules \(3, 4\))]TJ 0.0985 Tw 9.525 0 Td (. For this purpose, )Tj 0.00079 Tc 0.1449 Tw -28.46 -1.15 Td [(the BDD perform)8.6 (a)-0.4 (nce m)8.6 (a)-0.4 (y be i)-6.4 (m)8.6 (proved by de)]TJ 0.0007 Tc 0.1443 Tw 19.605 0 Td [(positing cop)5.7 (p)0.7 (er particles)4.9 ( on its surface,)5.7 ( )]TJ 0.0002 Tc 0.5598 Tw -19.605 -1.15 Td (which are responsible for its sensitivit)Tj 0.00011 Tc 18.005 0 Td (y and selectivity increasing the nitrate )Tj 0.00031 Tc 0 Tw -18.005 -1.15 Td (electroreducti)Tj 0.0005 Tc -0.00301 Tw 5.5 0 Td (on process \(5\).)Tj 0.535 g 0 Tc 0 Tw 10.02 0 0 10.02 226.92 204.2401 Tm ( )Tj 0 g 0.0005 Tc 0.10699 Tw 12 0 0 12 90 188.64 Tm (Several studies have )Tj 0.0002 Tc 0.1098 Tw 8.745 0 Td [(confirm)8 (e)-1 (d that the photo-assisted )3 (m)7.9 (e)-0.9 (tal deposition m)7.9 (e)-0.9 (thod is very )]TJ 0.0007 Tc 0.0043 Tw -8.745 -1.15 Td (useful for the preparation of )Tj 0.0009 Tc 0.0034 Tw 11.5 0 Td [(efficient electrode m)8.7 (a)-0.3 (terial \(6, 7\). Fujishim)8.7 (a)-0.3 ( and Honda)-5.2 ( have)-5.2 ( )]TJ 0 Tc 0.09779 Tw -11.5 -1.15 Td [(argued that one of the most prom)7.8 (inent featur)]TJ -0.00011 Tc 0.1001 Tw 18.54 0 Td [(es of sem)7.7 (i)-2.3 (conductors )]TJ 0 Tc 0.10001 Tw 8.985 0 Td (is their photoactivity )Tj 0.00079 Tc 0.12331 Tw -27.525 -1.15 Td [(\(8\). Am)8.6 (ong the sem)8.6 (i)-1.4 (conductors, the titanium)8.6 ( di)]TJ 0.00031 Tc 0.12379 Tw 19.75 0 Td (oxide has been widely exploited for its )Tj 0.0005 Tc 0.75281 Tw -19.75 -1.15 Td [(photochem)8.3 (i)-1.7 (cal properties, like m)8.3 (e)-0.7 (ta)]TJ 0.00031 Tc 0.7547 Tw 16.59 0 Td [(l photodeposition and organic com)8.1 (pound )]TJ 0.0005 Tc -0.0005 Tw -16.59 -1.15 Td [(decom)8.3 (position in contam)8.3 (inated waters \(9, )]TJ 0.0006 Tc -0.0022 Tw 17.005 0 Td [(10\). Conversely, the diam)8.4 (ond film has received)5.6 ( )]TJ 0.0009 Tc 0.02409 Tw -17.005 -1.15 Td [(less atten)5.9 (tio)5.9 (n, especially)5.9 ( with )]TJ 0.0006 Tc 0.0244 Tw 12.13 0 Td [(respect to the photoelectrodep)5.6 (o)0.6 (s)]TJ 0.02229 Tw 12.995 0 Td [(ition of metallic ions on its)4.9 ( )]TJ 0 Tw -25.125 -1.15 Td [(surface.)5.6 ( )]TJ 0.0002 Tc 0.0448 Tw T* [(The diam)8 (ond, in its natural st)]TJ -0.0002 Tc 0.0439 Tw 11.945 0 Td (ate, is considered a wide )Tj 0.0007 Tc 0.0405 Tw 10.27 0 Td [(band gap sem)8.5 (i)-1.5 (conductor \(5.5 eV\). )]TJ 0.0394 Tw -22.215 -1.15 Td [(Due to its extrem)8.4 (ely wide gap and its conduction band edge is located at a very negative \ )]TJ ET q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 220.17 773.38 Td (ECS Transactions, 43 \(1\) 177-183 \(2012\))Tj /GS1 gs -18.745 -11.667 Td (10.1149/1.4704955 \251 The Electrochemical Society)Tj ET Q q 0 0 612 792 re W n BT 0.2 g /GS1 gs /T1_0 10 Tf 0 Tc 0 Tw 298.5 12 Td (177)Tj ET Q BT /GS1 gs /T1_1 1 Tf 0 Tc 0 Tw 7 0 0 7 443.35738 13 Tm (\) unless CC License in place \(see abstract\).\240 )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -11.72697 0 Td (ecsdl.org/site/terms_use)Tj 0 g /GS1 gs /T1_1 1 Tf -25.67698 0 Td ( address. Redistribution subject to ECS terms of use \(see )Tj 0 0 1 rg /GS1 gs /T1_2 1 Tf -7.50599 0 Td (169.230.243.252)Tj 0 g /GS1 gs /T1_1 1 Tf -14.95299 0 Td (Downloaded on 2015-04-09 to IP )Tj ET endstream endobj 77 0 obj <> endobj 116 0 obj <> endobj 117 0 obj <> endobj 118 0 obj <> endobj 1 0 obj <> endobj 7 0 obj <<>> endobj 6 0 obj <> endobj 73 0 obj <> endobj xref 0 119 0000000000 65535 f 0000399274 00000 n 0000167119 00000 n 0000351541 00000 n 0000351751 00000 n 0000354486 00000 n 0000399318 00000 n 0000399298 00000 n 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000140031 00000 n 0000139346 00000 n 0000166488 00000 n 0000166804 00000 n 0000166577 00000 n 0000166209 00000 n 0000351463 00000 n 0000351507 00000 n 0000354442 00000 n 0000258910 00000 n 0000175860 00000 n 0000139818 00000 n 0000140243 00000 n 0000139620 00000 n 0000138878 00000 n 0000012170 00000 n 0000011093 00000 n 0000000000 00000 f 0000000000 00000 f 0000012409 00000 n 0000011925 00000 n 0000012844 00000 n 0000012648 00000 n 0000009151 00000 n 0000038002 00000 n 0000010389 00000 n 0000011494 00000 n 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000000000 00000 f 0000001782 00000 n 0000001833 00000 n 0000003804 00000 n 0000001687 00000 n 0000003482 00000 n 0000003148 00000 n 0000002762 00000 n 0000002451 00000 n 0000002162 00000 n 0000001884 00000 n 0000001652 00000 n 0000000156 00000 n 0000399502 00000 n 0000000016 00000 n 0000390647 00000 n 0000390681 00000 n 0000398958 00000 n 0000010206 00000 n 0000010295 00000 n 0000379007 00000 n 0000379041 00000 n 0000390331 00000 n 0000355015 00000 n 0000355049 00000 n 0000378691 00000 n 0000168254 00000 n 0000168288 00000 n 0000354699 00000 n 0000140765 00000 n 0000140799 00000 n 0000167938 00000 n 0000038369 00000 n 0000038403 00000 n 0000140449 00000 n 0000004093 00000 n 0000004125 00000 n 0000038055 00000 n 0000038092 00000 n 0000038203 00000 n 0000038304 00000 n 0000140486 00000 n 0000140598 00000 n 0000140700 00000 n 0000167975 00000 n 0000168087 00000 n 0000168189 00000 n 0000354736 00000 n 0000354848 00000 n 0000354950 00000 n 0000378728 00000 n 0000378840 00000 n 0000378942 00000 n 0000390368 00000 n 0000390480 00000 n 0000390582 00000 n 0000398995 00000 n 0000399107 00000 n 0000399209 00000 n trailer <]>> startxref 399682 %%EOF